Aethoxy-chlor-diphenyl-silan

Base Information

• Chemical Name: Aethoxy-chlor-diphenyl-silan
• CAS No.: 53668-80-7
• Molecular Formula: C₁₄H₁₅ClOSi
• Molecular Weight: 262.811
• Mol file: 53668-80-7.mol

Synonyms:Aethoxy-chlor-diphenyl-silan

Chemical Property of Aethoxy-chlor-diphenyl-silan

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Aethoxy-chlor-diphenyl-silan

There total 5 articles about Aethoxy-chlor-diphenyl-silan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

ethoxy(diphenyl)silane (18407-46-0) → Aethoxy-chlor-diphenyl-silan (53668-80-7)

Guidance literature:

With tetrachloromethane; palladium dichloride; In toluene; at 25 ℃; for 15h;

DOI:10.1016/j.jorganchem.2004.07.048

Reference yield:

diethyl ether (60-29-7,927820-24-4) + diphenylsilyl chloride (1631-83-0) → Aethoxy-chlor-diphenyl-silan (53668-80-7)

Guidance literature:

With ether adduct of tris(pentafluorophenyl)boron; In toluene; at 20 ℃; for 1h; Inert atmosphere; Schlenk technique;

DOI:10.1002/anie.201700324

Reference yield:

diphenylsilane (775-12-2) → Aethoxy-chlor-diphenyl-silan (53668-80-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 65 percent / PdCl₂ / benzene / 24 h / 25 °C

2: 79 percent / PdCl₂; CCl₄ / toluene / 15 h / 25 °C

With tetrachloromethane; palladium dichloride; In toluene; benzene;

DOI:10.1016/j.jorganchem.2004.07.048

upstream raw materials:

ethanol

diphenylsilyl dichloride

ethoxy(diphenyl)silane

diphenylsilane

Downstream raw materials:

4,4'-Bis-(ethoxydiphenylsilyl)-biphenyl

Butyl-ethoxy-diphenyl-silane

1,4-phenylenebis(diphenylsilanol)

(ethoxy)diphenyl(vinyl)silane

Refernces

• 1、 Ohshita, Joji,Taketsugu, Ryosuke,Nakahara, Yuki,Kunai, Atsutaka. "Convenient synthesis of alkoxyhalosilanes from hydrosilanes". . p. 3258 - 3264. Retrieved 2007/10/03.