4-(2,4-Dichloro-benzoylamino)-2-phenyl-thiazole-5-carboxylic acid t-butyl ester

Base Information

• Chemical Name: 4-(2,4-Dichloro-benzoylamino)-2-phenyl-thiazole-5-carboxylic acid t-butyl ester
• CAS No.: 548458-71-5
• Molecular Formula: C₂₁H₁₈Cl₂N₂O₃S
• Molecular Weight: 449.358

Synonyms:4-(2,4-Dichloro-benzoylamino)-2-phenyl-thiazole-5-carboxylic acid t-butyl ester

Chemical Property of 4-(2,4-Dichloro-benzoylamino)-2-phenyl-thiazole-5-carboxylic acid t-butyl ester

Chemical Property:

Purity/Quality:

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Technology Process of 4-(2,4-Dichloro-benzoylamino)-2-phenyl-thiazole-5-carboxylic acid t-butyl ester

There total 1 articles about 4-(2,4-Dichloro-benzoylamino)-2-phenyl-thiazole-5-carboxylic acid t-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

aqueous lithium hydroxide + methanol-THF + 4-Amino-2-phenyl-thiazole-5-carboxylic acid t-butyl ester (548458-68-0) + 2,4-dichlorobenzoyl chloride (89-75-8) → 4-(2,4-Dichloro-benzoylamino)-2-phenyl-thiazole-5-carboxylic acid t-butyl ester (548458-71-5)

Guidance literature:

With NaH; acetic acid; In hexane; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

4-(2,4-Dichloro-benzoylamino)-2-phenyl-thiazole-5-carboxylic acid t-butyl ester (548458-71-5) + methyl iodide (74-88-4) → 4-[(2,4-dichloro-benzoyl)-methyl-amino]-2-phenyl-thiazole-5-carboxylic acid t-butyl ester (548458-72-6)

Guidance literature:

With NaH; In hexane; ethyl acetate; N,N-dimethyl-formamide;

upstream raw materials:

4-Amino-2-phenyl-thiazole-5-carboxylic acid t-butyl ester

2,4-dichlorobenzoyl chloride

Downstream raw materials:

4-[(2,4-dichloro-benzoyl)-methyl-amino]-2-phenyl-thiazole-5-carboxylic acid t-butyl ester

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