<2'-(Phenylselenenyl)-ethyl>-4,6-di-O-acetyl-2,3-dideoxy-α-D-erythro-hexenopyranoside

Base Information

Chemical Name:<2'-(Phenylselenenyl)-ethyl>-4,6-di-O-acetyl-2,3-dideoxy-α-D-erythro-hexenopyranoside
CAS No.:89755-42-0
Molecular Formula:C₁₈H₂₂O₆Se
Molecular Weight:413.329
Hs Code.:

Synonyms:<2'-(Phenylselenenyl)-ethyl>-4,6-di-O-acetyl-2,3-dideoxy-α-D-erythro-hexenopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of <2'-(Phenylselenenyl)-ethyl>-4,6-di-O-acetyl-2,3-dideoxy-α-D-erythro-hexenopyranoside

Chemical Property:

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Technology Process of <2'-(Phenylselenenyl)-ethyl>-4,6-di-O-acetyl-2,3-dideoxy-α-D-erythro-hexenopyranoside

There total 2 articles about <2'-(Phenylselenenyl)-ethyl>-4,6-di-O-acetyl-2,3-dideoxy-α-D-erythro-hexenopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 65275-32-3
2-(phenylselenyl)ethanol

: 2873-29-2
D-glucal triacetate

: 89755-42-0
<2'-(Phenylselenenyl)-ethyl>-4,6-di-O-acetyl-2,3-dideoxy-α-D-erythro-hexenopyranoside

Guidance literature:: With boron trifluoride diethyl etherate; In benzene; at 0 - 25 ℃; for 0.0833333h; Inert atmosphere;
DOI:10.1002/ejoc.201200898

Reference yield:

: 1666-13-3
diphenyl diselenide

: 89755-42-0
<2'-(Phenylselenenyl)-ethyl>-4,6-di-O-acetyl-2,3-dideoxy-α-D-erythro-hexenopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / NaBH₄ / ethanol / 0.5 h / -20 °C

2: 85 percent / BF₃*Et₂O / benzene / 0.25 h

With sodium tetrahydroborate; boron trifluoride diethyl etherate; In ethanol; benzene;
DOI:10.1055/s-1984-30752

Reference yield:

: 89755-42-0
<2'-(Phenylselenenyl)-ethyl>-4,6-di-O-acetyl-2,3-dideoxy-α-D-erythro-hexenopyranoside

: 1581704-97-3
2-phenylselenenylethyl 4,6-di-O-benzyl-2,3-dideoxy-α-D-erythrohex-2-enopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: methanol; potassium carbonate / 3 h / Inert atmosphere

2.1: sodium hydride / tetrahydrofuran / 1.33 h / 0 °C / Inert atmosphere

2.2: 25 °C / Inert atmosphere

With methanol; sodium hydride; potassium carbonate; In tetrahydrofuran;
DOI:10.1002/ejoc.201301665