C₄₉H₆₀N₃O₅P

Base Information

Chemical Name:C₄₉H₆₀N₃O₅P
CAS No.:1394941-00-4
Molecular Formula:C₄₉H₆₀N₃O₅P
Molecular Weight:802.006
Hs Code.:

C<sub>49</sub>H<sub>60</sub>N<sub>3</sub>O<sub>5</sub>P

Synonyms:C₄₉H₆₀N₃O₅P

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Chemical Property of C₄₉H₆₀N₃O₅P

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Technology Process of C₄₉H₆₀N₃O₅P

There total 4 articles about C₄₉H₆₀N₃O₅P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1394940-80-7
C₅₇H₆₆N₃O₇P

: 1394941-00-4
C₄₉H₆₀N₃O₅P

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol;
DOI:10.1016/j.bmcl.2012.07.011

Reference yield:

: 102560-84-9
4-hydroxy-N-tritylbutanamide

: 1394941-00-4
C₄₉H₆₀N₃O₅P

Guidance literature:: Multi-step reaction with 5 steps

1.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 2.25 h / -60 °C

2.1: trichlorophosphate / acetonitrile / 6 h / Reflux

2.2: 4 h / Reflux

3.1: palladium 10% on activated carbon; hydrogen / methanol

4.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine / acetonitrile / 20 °C

5.1: palladium 10% on activated carbon; hydrogen / methanol

With oxalyl dichloride; palladium 10% on activated carbon; hydrogen; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; dimethyl sulfoxide; triethylamine; trichlorophosphate; In methanol; dichloromethane; acetonitrile; 1.1: Swern oxidation / 1.2: Swern oxidation;
DOI:10.1016/j.bmcl.2012.07.011

Reference yield:

: 1195771-44-8
methyl 4-oxo-4-(tritylamino)butanoate

: 1394941-00-4
C₄₉H₆₀N₃O₅P

Guidance literature:: Multi-step reaction with 6 steps

1.1: lithium borohydride / tetrahydrofuran; ethanol / 20 °C

2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 2.25 h / -60 °C

3.1: trichlorophosphate / acetonitrile / 6 h / Reflux

3.2: 4 h / Reflux

4.1: palladium 10% on activated carbon; hydrogen / methanol

5.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine / acetonitrile / 20 °C

6.1: palladium 10% on activated carbon; hydrogen / methanol

With lithium borohydride; oxalyl dichloride; palladium 10% on activated carbon; hydrogen; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; dimethyl sulfoxide; triethylamine; trichlorophosphate; In tetrahydrofuran; methanol; ethanol; dichloromethane; acetonitrile; 2.1: Swern oxidation / 2.2: Swern oxidation;
DOI:10.1016/j.bmcl.2012.07.011