C₁₇H₁₆F₃NO₂

Base Information

Chemical Name:C₁₇H₁₆F₃NO₂
CAS No.:1380243-43-5
Molecular Formula:C₁₇H₁₆F₃NO₂
Molecular Weight:323.315
Hs Code.:

C<sub>17</sub>H<sub>16</sub>F<sub>3</sub>NO<sub>2</sub>

Synonyms:C₁₇H₁₆F₃NO₂

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Chemical Property of C₁₇H₁₆F₃NO₂

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Technology Process of C₁₇H₁₆F₃NO₂

There total 6 articles about C₁₇H₁₆F₃NO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1380243-31-1
C₁₈H₁₈F₃NOS

: 1380243-43-5
C₁₇H₁₆F₃NO₂

Guidance literature:: C₁₈H₁₈F₃NOS; With methyl iodide; In methanol; water; at 20 ℃; for 0.5h; Cooling with ice;

With water; sodium hydrogencarbonate; pH=3 - Ca. 7; Reflux;

Reference yield:

: 10290-61-6
(S)-N-benzoylmethionine

: 1380243-43-5
C₁₇H₁₆F₃NO₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium tetrahydroborate; iodine; methanol / tetrahydrofuran / 2 h / 0 - 5 °C / Reflux

2.1: triethylamine / dichloromethane / 4 h / 0 - 20 °C

3.1: sodium hydride / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere

4.1: isopropylmagnesium bromide / tetrahydrofuran / -20 °C / Inert atmosphere

4.2: 0.25 h / -5 °C / Inert atmosphere

4.3: 0.08 h

5.1: methyl iodide / water; methanol / 0.5 h / 20 °C / Cooling with ice

5.2: pH 3 - Ca_. 7 / Reflux

With methanol; sodium tetrahydroborate; iodine; isopropylmagnesium bromide; sodium hydride; triethylamine; methyl iodide; In tetrahydrofuran; methanol; dichloromethane; water;

Reference yield:

: 1303536-70-0
(S)-N-[1-hydroxy-4-(methylthio)butan-2-yl]benzamide

: 1380243-43-5
C₁₇H₁₆F₃NO₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine / dichloromethane / 4 h / 0 - 20 °C

2.1: sodium hydride / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere

3.1: isopropylmagnesium bromide / tetrahydrofuran / -20 °C / Inert atmosphere

3.2: 0.25 h / -5 °C / Inert atmosphere

3.3: 0.08 h

4.1: methyl iodide / water; methanol / 0.5 h / 20 °C / Cooling with ice

4.2: pH 3 - Ca_. 7 / Reflux

With isopropylmagnesium bromide; sodium hydride; triethylamine; methyl iodide; In tetrahydrofuran; methanol; dichloromethane; water;