C₁₉H₁₅NO₄S

Base Information

Chemical Name:C₁₉H₁₅NO₄S
CAS No.:1423700-86-0
Molecular Formula:C₁₉H₁₅NO₄S
Molecular Weight:353.398
Hs Code.:

C<sub>19</sub>H<sub>15</sub>NO<sub>4</sub>S

Synonyms:C₁₉H₁₅NO₄S

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Chemical Property of C₁₉H₁₅NO₄S

Chemical Property:

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Technology Process of C₁₉H₁₅NO₄S

There total 7 articles about C₁₉H₁₅NO₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1423700-84-8
C₂₅H₂₇NO₄S

: 1423700-86-0
C₁₉H₁₅NO₄S

Guidance literature:: C₂₅H₂₇NO₄S; With sodium hydroxide; In tetrahydrofuran; methanol; at 20 ℃;

With hydrogenchloride; In tetrahydrofuran; methanol; water; at 0 ℃; pH=4.0;

Reference yield:

: 29203-58-5
4-bromo-N-hydroxybenzenecarboximidoyl chloride

: 1423700-86-0
C₁₉H₁₅NO₄S

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium methylate / methanol / 0.67 h / 0 - 25 °C

2.1: potassium phosphate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / water; 1,2-dimethoxyethane / 5 h / 80 °C

3.1: hydrogen / ethanol / 3 h / 20 °C

4.1: Lawessons reagent / dichloromethane / 20 °C

4.2: 24 h

5.1: sodium hydroxide / methanol; tetrahydrofuran / 20 °C

5.2: 0 °C / pH 4.0

With Lawessons reagent; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate; hydrogen; sodium methylate; sodium hydroxide; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; ethanol; dichloromethane; water;

Reference yield:

: 25062-46-8,40979-16-6,34158-73-1
4-bromobenzaldehyde oxime

: 1423700-86-0
C₁₉H₁₅NO₄S

Guidance literature:: Multi-step reaction with 6 steps

1.1: N-chloro-succinimide / N,N-dimethyl-formamide / 2 h / 15 - 20 °C

2.1: sodium methylate / methanol / 0.67 h / 0 - 25 °C

3.1: potassium phosphate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / water; 1,2-dimethoxyethane / 5 h / 80 °C

4.1: hydrogen / ethanol / 3 h / 20 °C

5.1: Lawessons reagent / dichloromethane / 20 °C

5.2: 24 h

6.1: sodium hydroxide / methanol; tetrahydrofuran / 20 °C

6.2: 0 °C / pH 4.0

With Lawessons reagent; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate; N-chloro-succinimide; hydrogen; sodium methylate; sodium hydroxide; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; ethanol; dichloromethane; water; N,N-dimethyl-formamide;