4-Benzyloxy-3-(p-tolylsulfonylmethyl)-1-<2-(tert.-butylamino)-1-hydroxy-aethyl>-benzol

Base Information

Chemical Name:4-Benzyloxy-3-(p-tolylsulfonylmethyl)-1-<2-(tert.-butylamino)-1-hydroxy-aethyl>-benzol
CAS No.:779267-91-3
Molecular Formula:C₂₇H₃₃NO₄S
Molecular Weight:467.629
Hs Code.:

Synonyms:4-Benzyloxy-3-(p-tolylsulfonylmethyl)-1-<2-(tert.-butylamino)-1-hydroxy-aethyl>-benzol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-Benzyloxy-3-(p-tolylsulfonylmethyl)-1-<2-(tert.-butylamino)-1-hydroxy-aethyl>-benzol

Chemical Property:

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Technology Process of 4-Benzyloxy-3-(p-tolylsulfonylmethyl)-1-<2-(tert.-butylamino)-1-hydroxy-aethyl>-benzol

There total 6 articles about 4-Benzyloxy-3-(p-tolylsulfonylmethyl)-1-<2-(tert.-butylamino)-1-hydroxy-aethyl>-benzol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 340173-17-3
4-Benzyloxy-3-(p-tolylsulfonylmethyl)-ω-(tert-butylimino)-acetophenon

: 779267-91-3
4-Benzyloxy-3-(p-tolylsulfonylmethyl)-1-<2-(tert.-butylamino)-1-hydroxy-aethyl>-benzol

Guidance literature:: With sodium tetrahydroborate; In ethanol;
DOI:10.1021/jm00241a006

Reference yield:

: 24085-05-0
1-(3-chloromethyl-4-hydroxyphenyl)ethanone

: 779267-91-3
4-Benzyloxy-3-(p-tolylsulfonylmethyl)-1-<2-(tert.-butylamino)-1-hydroxy-aethyl>-benzol

Guidance literature:: Multi-step reaction with 6 steps

1: methanol; H₂O / Heating

2: aq. K₂CO₃, NaI / acetone

3: pyrrolidin-2-one hydrotribromide, pyrrolidin-2-one / tetrahydrofuran / Heating

4: dimethylsulfoxide

5: methanol

6: NaBH₄ / ethanol

With 2-pyrrolidinon; sodium tetrahydroborate; pyrrolidone hydrotribromide; potassium carbonate; sodium iodide; In tetrahydrofuran; methanol; ethanol; water; dimethyl sulfoxide; acetone;
DOI:10.1021/jm00241a006

Reference yield:

: 56490-65-4
1-[4-Hydroxy-3-(toluene-4-sulfonylmethyl)-phenyl]-ethanone

: 779267-91-3
4-Benzyloxy-3-(p-tolylsulfonylmethyl)-1-<2-(tert.-butylamino)-1-hydroxy-aethyl>-benzol

Guidance literature:: Multi-step reaction with 5 steps

1: aq. K₂CO₃, NaI / acetone

2: pyrrolidin-2-one hydrotribromide, pyrrolidin-2-one / tetrahydrofuran / Heating

3: dimethylsulfoxide

4: methanol

5: NaBH₄ / ethanol

With 2-pyrrolidinon; sodium tetrahydroborate; pyrrolidone hydrotribromide; potassium carbonate; sodium iodide; In tetrahydrofuran; methanol; ethanol; dimethyl sulfoxide; acetone;
DOI:10.1021/jm00241a006