N-[(2R,3R,4S,6R)-4-Benzyloxy-6-hydroxymethyl-6-p-tolylsulfanyl-2-((1S,2R)-1,2,3-tris-benzyloxy-propyl)-tetrahydro-pyran-3-yl]-acetamide

Base Information

Chemical Name:N-[(2R,3R,4S,6R)-4-Benzyloxy-6-hydroxymethyl-6-p-tolylsulfanyl-2-((1S,2R)-1,2,3-tris-benzyloxy-propyl)-tetrahydro-pyran-3-yl]-acetamide
CAS No.:358681-53-5
Molecular Formula:C₄₆H₅₁NO₇S
Molecular Weight:761.979
Hs Code.:

Synonyms:N-[(2R,3R,4S,6R)-4-Benzyloxy-6-hydroxymethyl-6-p-tolylsulfanyl-2-((1S,2R)-1,2,3-tris-benzyloxy-propyl)-tetrahydro-pyran-3-yl]-acetamide

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Chemical Property of N-[(2R,3R,4S,6R)-4-Benzyloxy-6-hydroxymethyl-6-p-tolylsulfanyl-2-((1S,2R)-1,2,3-tris-benzyloxy-propyl)-tetrahydro-pyran-3-yl]-acetamide

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Technology Process of N-[(2R,3R,4S,6R)-4-Benzyloxy-6-hydroxymethyl-6-p-tolylsulfanyl-2-((1S,2R)-1,2,3-tris-benzyloxy-propyl)-tetrahydro-pyran-3-yl]-acetamide

There total 6 articles about N-[(2R,3R,4S,6R)-4-Benzyloxy-6-hydroxymethyl-6-p-tolylsulfanyl-2-((1S,2R)-1,2,3-tris-benzyloxy-propyl)-tetrahydro-pyran-3-yl]-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 358681-52-4
(2R,4S,5R,6R)-5-Acetylamino-4-benzyloxy-2-p-tolylsulfanyl-6-((1S,2R)-1,2,3-tris-benzyloxy-propyl)-tetrahydro-pyran-2-carboxylic acid benzyl ester

: 358681-53-5
N-[(2R,3R,4S,6R)-4-Benzyloxy-6-hydroxymethyl-6-p-tolylsulfanyl-2-((1S,2R)-1,2,3-tris-benzyloxy-propyl)-tetrahydro-pyran-3-yl]-acetamide

Guidance literature:: With lithium borohydride; In tetrahydrofuran; methanol;
DOI:10.1039/b102166b

Reference yield:

: 100-39-0
benzyl bromide

: 358681-53-5
N-[(2R,3R,4S,6R)-4-Benzyloxy-6-hydroxymethyl-6-p-tolylsulfanyl-2-((1S,2R)-1,2,3-tris-benzyloxy-propyl)-tetrahydro-pyran-3-yl]-acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 55 percent / NaH / dimethylformamide

2: 90 percent / LiBH₄ / tetrahydrofuran; methanol

With lithium borohydride; sodium hydride; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1039/b102166b

Reference yield:

: 6931-68-6,72690-21-2,74006-95-4,108740-37-0,108740-38-1,108740-39-2,119241-63-3,119241-64-4,119241-65-5,147129-72-4,147129-73-5,73208-82-9
methyl 5-acetamido-2,4,7,8,9-penta-O-acetyl-3,5-dideoxy-D-glycero-D-galacto-2-nonulopyranosonate

: 358681-53-5
N-[(2R,3R,4S,6R)-4-Benzyloxy-6-hydroxymethyl-6-p-tolylsulfanyl-2-((1S,2R)-1,2,3-tris-benzyloxy-propyl)-tetrahydro-pyran-3-yl]-acetamide

Guidance literature:: Multi-step reaction with 4 steps

1: 75 percent / BF₃*Et₂O / CH₂Cl₂

2: 100 percent / NaOMe / methanol

3: 55 percent / NaH / dimethylformamide

4: 90 percent / LiBH₄ / tetrahydrofuran; methanol

With lithium borohydride; boron trifluoride diethyl etherate; sodium methylate; sodium hydride; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/b102166b