Diisopropyl-carbamic acid (R)-1-(1-hydroxy-cyclohex-2-enyl)-3-phenyl-propyl ester

Base Information

Chemical Name:Diisopropyl-carbamic acid (R)-1-(1-hydroxy-cyclohex-2-enyl)-3-phenyl-propyl ester
CAS No.:350589-34-3
Molecular Formula:C₂₂H₃₃NO₃
Molecular Weight:359.509
Hs Code.:

Synonyms:Diisopropyl-carbamic acid (R)-1-(1-hydroxy-cyclohex-2-enyl)-3-phenyl-propyl ester

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Chemical Property of Diisopropyl-carbamic acid (R)-1-(1-hydroxy-cyclohex-2-enyl)-3-phenyl-propyl ester

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Technology Process of Diisopropyl-carbamic acid (R)-1-(1-hydroxy-cyclohex-2-enyl)-3-phenyl-propyl ester

There total 2 articles about Diisopropyl-carbamic acid (R)-1-(1-hydroxy-cyclohex-2-enyl)-3-phenyl-propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 930-68-7
cyclohexenone

: 475301-87-2,871941-32-1,246021-86-3
(1S)-3-phenyl-1-(tributylstannyl)propyl diisopropylcarbamate

: C₁₆H₂₄⁽²⁾HNO₂

: 350589-34-3
Diisopropyl-carbamic acid (R)-1-(1-hydroxy-cyclohex-2-enyl)-3-phenyl-propyl ester

Guidance literature:: Multistep reaction;
DOI:10.1016/S0022-328X(01)00641-6

Reference yield: 44.0%

: 930-68-7
cyclohexenone

: 475301-87-2,871941-32-1,246021-86-3
(1S)-3-phenyl-1-(tributylstannyl)propyl diisopropylcarbamate

: 350589-34-3
Diisopropyl-carbamic acid (R)-1-(1-hydroxy-cyclohex-2-enyl)-3-phenyl-propyl ester

Guidance literature:: (1S)-3-phenyl-1-(tributylstannyl)propyl diisopropylcarbamate; With n-butyllithium; In tetrahydrofuran; at -78 ℃;

With magnesium bromide; In tetrahydrofuran; at -78 ℃; for 1h;

cyclohexenone; In tetrahydrofuran; at 20 ℃; for 1h;
DOI:10.1016/S0022-328X(01)00641-6