1-Phenyl-12-piperidino-13-oxa-3-azatetracyclo<5.5.2.0^3.7.0^8.12>tetradecan-2,14-dion

Base Information

• Chemical Name: 1-Phenyl-12-piperidino-13-oxa-3-azatetracyclo<5.5.2.0^3.7.0^8.12>tetradecan-2,14-dion
• CAS No.: 112423-24-2
• Molecular Formula: C₂₃H₂₈N₂O₃
• Molecular Weight: 380.487

Synonyms:1-Phenyl-12-piperidino-13-oxa-3-azatetracyclo<5.5.2.0^3.7.0^8.12>tetradecan-2,14-dion

Chemical Property of 1-Phenyl-12-piperidino-13-oxa-3-azatetracyclo<5.5.2.0^3.7.0^8.12>tetradecan-2,14-dion

Chemical Property:

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Technology Process of 1-Phenyl-12-piperidino-13-oxa-3-azatetracyclo<5.5.2.0^3.7.0^8.12>tetradecan-2,14-dion

There total 2 articles about 1-Phenyl-12-piperidino-13-oxa-3-azatetracyclo<5.5.2.0^3.7.0^8.12>tetradecan-2,14-dion which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

1-(N-piperidino)cyclopentene (1614-92-2) + 7,8-Dihydro-2-oxo-3-phenyl-2H,6H-pyrrolo<2,1-b><1,3>oxazin-5-ium-4-olat (81685-04-3) → 1-Phenyl-12-piperidino-13-oxa-3-azatetracyclo<5.5.2.03.7.08.12>tetradecan-2,14-dion (112423-24-2)

Guidance literature:

In dichloromethane; for 0.166667h; Ambient temperature;

Reference yield:

(chlorocarbonyl)phenyl ketene (17118-70-6) → 1-Phenyl-12-piperidino-13-oxa-3-azatetracyclo<5.5.2.03.7.08.12>tetradecan-2,14-dion (112423-24-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 95 percent / ethyl acetate / Ambient temperature

2: 73 percent / CH₂Cl₂ / 0.17 h / Ambient temperature

In dichloromethane; ethyl acetate;

Reference yield: 83.0%

1-Phenyl-12-piperidino-13-oxa-3-azatetracyclo<5.5.2.03.7.08.12>tetradecan-2,14-dion (112423-24-2) → 1,2,3,7,8,9-Hexahydro-6-phenyl-5H-cyclopentaindolizin-5-on (112423-29-7)

Guidance literature:

With toluene-4-sulfonic acid; In dichloromethane; for 2h; Ambient temperature;

upstream raw materials:

1-(N-piperidino)cyclopentene

7,8-Dihydro-2-oxo-3-phenyl-2H,6H-pyrrolo<2,1-b><1,3>oxazin-5-ium-4-olat

(chlorocarbonyl)phenyl ketene

Downstream raw materials:

1,2,3,7,8,9-Hexahydro-6-phenyl-5H-cyclopentaindolizin-5-on

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