(1S,1'S)-1,1'-(1-benzoyl-1H-1,2,4-triazole-3,5-diyl)-bis(ethane-1,1-diyl) dibenzoate

Base Information

Chemical Name:(1S,1'S)-1,1'-(1-benzoyl-1H-1,2,4-triazole-3,5-diyl)-bis(ethane-1,1-diyl) dibenzoate
CAS No.:1176540-37-6
Molecular Formula:C₂₇H₂₃N₃O₅
Molecular Weight:469.497
Hs Code.:

Synonyms:(1S,1'S)-1,1'-(1-benzoyl-1H-1,2,4-triazole-3,5-diyl)-bis(ethane-1,1-diyl) dibenzoate

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Chemical Property of (1S,1'S)-1,1'-(1-benzoyl-1H-1,2,4-triazole-3,5-diyl)-bis(ethane-1,1-diyl) dibenzoate

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Technology Process of (1S,1'S)-1,1'-(1-benzoyl-1H-1,2,4-triazole-3,5-diyl)-bis(ethane-1,1-diyl) dibenzoate

There total 1 articles about (1S,1'S)-1,1'-(1-benzoyl-1H-1,2,4-triazole-3,5-diyl)-bis(ethane-1,1-diyl) dibenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 98-88-4
benzoyl chloride

: 111853-55-5
(S,S)-3,5-bis(1-hydroxyethyl)-1H-1,2,4-triazole

: 1176540-37-6
(1S,1'S)-1,1'-(1-benzoyl-1H-1,2,4-triazole-3,5-diyl)-bis(ethane-1,1-diyl) dibenzoate

Guidance literature:: With triethylamine; In tetrahydrofuran; at 20 ℃; for 12h;
DOI:10.1016/j.tetasy.2009.12.007

Reference yield:

: 1176540-37-6
(1S,1'S)-1,1'-(1-benzoyl-1H-1,2,4-triazole-3,5-diyl)-bis(ethane-1,1-diyl) dibenzoate

: 15028-40-7,13226-98-7
DL-2-phenylglycine methyl ester hydrochloride

: 62045-88-9,81912-50-7,119817-55-9,73521-11-6
methyl (R)-2-benzoylamino-2-phenylacetate

: 81912-50-7
(S)-benzoylamino-phenyl-acetic acid methyl ester

Guidance literature:: DL-2-phenylglycine methyl ester hydrochloride; With triethylamine; In tetrahydrofuran; at 20 ℃;

(1S,1'S)-1,1'-(1-benzoyl-1H-1,2,4-triazole-3,5-diyl)-bis(ethane-1,1-diyl) dibenzoate; In tetrahydrofuran; at 25 ℃; enantioselective reaction;
DOI:10.1016/j.tetasy.2009.12.007