{5-Chloro-2-[2-(4-chloro-phenyl)-2-oxo-ethoxy]-benzyl}-triphenyl-phosphonium; bromide

Base Information

Chemical Name:{5-Chloro-2-[2-(4-chloro-phenyl)-2-oxo-ethoxy]-benzyl}-triphenyl-phosphonium; bromide
CAS No.:109790-44-5
Molecular Formula:Br*C₃₃H₂₆Cl₂O₂P
Molecular Weight:636.352
Hs Code.:

Synonyms:{5-Chloro-2-[2-(4-chloro-phenyl)-2-oxo-ethoxy]-benzyl}-triphenyl-phosphonium; bromide

Suppliers and Price of {5-Chloro-2-[2-(4-chloro-phenyl)-2-oxo-ethoxy]-benzyl}-triphenyl-phosphonium; bromide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of {5-Chloro-2-[2-(4-chloro-phenyl)-2-oxo-ethoxy]-benzyl}-triphenyl-phosphonium; bromide

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of {5-Chloro-2-[2-(4-chloro-phenyl)-2-oxo-ethoxy]-benzyl}-triphenyl-phosphonium; bromide

There total 2 articles about {5-Chloro-2-[2-(4-chloro-phenyl)-2-oxo-ethoxy]-benzyl}-triphenyl-phosphonium; bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 6399-81-1
triphenylphosphine hydrobromide

: 109790-50-3
2-(4-Chloro-2-hydroxymethyl-phenoxy)-1-(4-chloro-phenyl)-ethanone

: 109790-44-5
{5-Chloro-2-[2-(4-chloro-phenyl)-2-oxo-ethoxy]-benzyl}-triphenyl-phosphonium; bromide

Guidance literature:: In acetonitrile; at 90 ℃; for 3h;
DOI:10.1016/0223-5234(87)90005-5

Reference yield:

: 536-38-9
4-chlorobenzoylmethyl bromide

: 109790-44-5
{5-Chloro-2-[2-(4-chloro-phenyl)-2-oxo-ethoxy]-benzyl}-triphenyl-phosphonium; bromide

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / K₂CO₃ / acetone / 3 h / 80 °C

2: 95 percent / acetonitrile / 3 h / 90 °C

With potassium carbonate; In acetone; acetonitrile;
DOI:10.1016/0223-5234(87)90005-5