(S)-1,1,1-trifluoro-2-(N-(R)-tert-butanesulfinyl)-amino-2-cyano-2-phenyl-ethane

Base Information

Chemical Name:(S)-1,1,1-trifluoro-2-(N-(R)-tert-butanesulfinyl)-amino-2-cyano-2-phenyl-ethane
CAS No.:884596-04-7
Molecular Formula:C₁₃H₁₅F₃N₂OS
Molecular Weight:304.336
Hs Code.:

Synonyms:(S)-1,1,1-trifluoro-2-(N-(R)-tert-butanesulfinyl)-amino-2-cyano-2-phenyl-ethane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-1,1,1-trifluoro-2-(N-(R)-tert-butanesulfinyl)-amino-2-cyano-2-phenyl-ethane

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Technology Process of (S)-1,1,1-trifluoro-2-(N-(R)-tert-butanesulfinyl)-amino-2-cyano-2-phenyl-ethane

There total 3 articles about (S)-1,1,1-trifluoro-2-(N-(R)-tert-butanesulfinyl)-amino-2-cyano-2-phenyl-ethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 2-Methyl-propane-2-sulfinic acid [2,2,2-trifluoro-1-phenyl-eth-(E)-ylidene]-amide

: 7677-24-9
trimethylsilyl cyanide

: 884596-04-7
(S)-1,1,1-trifluoro-2-(N-(R)-tert-butanesulfinyl)-amino-2-cyano-2-phenyl-ethane

Guidance literature:: In hexane; at 20 ℃; for 24h;
DOI:10.1021/ol0601186

Reference yield:

: 434-45-7
2,2,2-Trifluoroacetophenone

: 884596-04-7
(S)-1,1,1-trifluoro-2-(N-(R)-tert-butanesulfinyl)-amino-2-cyano-2-phenyl-ethane

Guidance literature:: Multi-step reaction with 2 steps

1: 58 percent Spectr_. / Ti(Oi-Pr)4 / hexane / 4 h / 20 °C

2: dimethylformamide / 12 h / -35 °C

With titanium(IV) isopropylate; In hexane; N,N-dimethyl-formamide; 2: Strecker asymmetric reaction;
DOI:10.1021/ol0601186