3-O-benzoyl-6-O-tert-butyldiphenylsilyl-1,2-O-isopropylidene-α-D-allofuranose

Base Information

Chemical Name:3-O-benzoyl-6-O-tert-butyldiphenylsilyl-1,2-O-isopropylidene-α-D-allofuranose
CAS No.:140451-81-6
Molecular Formula:C₃₂H₃₈O₇Si
Molecular Weight:562.735
Hs Code.:

Synonyms:3-O-benzoyl-6-O-tert-butyldiphenylsilyl-1,2-O-isopropylidene-α-D-allofuranose

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-O-benzoyl-6-O-tert-butyldiphenylsilyl-1,2-O-isopropylidene-α-D-allofuranose

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Technology Process of 3-O-benzoyl-6-O-tert-butyldiphenylsilyl-1,2-O-isopropylidene-α-D-allofuranose

There total 1 articles about 3-O-benzoyl-6-O-tert-butyldiphenylsilyl-1,2-O-isopropylidene-α-D-allofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.8%

: 31795-15-0
3-O-benzoyl-1,2-O-isopropylidene-α-D-allofuranose

: 58479-61-1
tert-butylchlorodiphenylsilane

: 140451-81-6
3-O-benzoyl-6-O-tert-butyldiphenylsilyl-1,2-O-isopropylidene-α-D-allofuranose

Guidance literature:: With pyridine; dmap; for 3.5h; Ambient temperature;
DOI:10.1016/0008-6215(92)80024-U

Reference yield: 92.9%

: 124-63-0
methanesulfonyl chloride

: 140451-81-6
3-O-benzoyl-6-O-tert-butyldiphenylsilyl-1,2-O-isopropylidene-α-D-allofuranose

: 140475-67-8
3-O-benzoyl-6-O-tert-butyldiphenylsilyl-1,2-O-isopropylidene-5-O-methanesulphonyl-α-D-allofuranose

Guidance literature:: With pyridine; at 0 ℃; for 2h;
DOI:10.1016/0008-6215(92)80024-U

Reference yield:

: 140451-81-6
3-O-benzoyl-6-O-tert-butyldiphenylsilyl-1,2-O-isopropylidene-α-D-allofuranose

: 140451-82-7
3-O-benzoyl-5-bromo-6-O-tert-butyldiphenylsilyl-5-deoxy-1,2-O-isopropylidene-α-D-allofuranose

Guidance literature:: Multi-step reaction with 2 steps

1: 92.9 percent / pyridine / 2 h / 0 °C

2: 24.9 percent / KBr, activated alumina, 18-crown-6 / dimethylformamide / 168 h / 90 - 100 °C

With pyridine; aluminum oxide; 18-crown-6 ether; potassium bromide; In N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(92)80024-U