ethyl 2-{[(phenylcarbonyl)carbamothioyl]amino}-4,5,6,7-tetrahydro-1-benzothiophene-3-carboxylate

Base Information

Chemical Name:ethyl 2-{[(phenylcarbonyl)carbamothioyl]amino}-4,5,6,7-tetrahydro-1-benzothiophene-3-carboxylate
CAS No.:53162-41-7
Molecular Formula:C₁₉H₂₀N₂O₃S₂
Molecular Weight:388.511
Hs Code.:
Mol file:53162-41-7.mol

Synonyms:ethyl 2-(3-benzoylthioureido)-4,5,6,7-tetrahydrobenzo[b]thiophene-3-carboxylate

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Chemical Property of ethyl 2-{[(phenylcarbonyl)carbamothioyl]amino}-4,5,6,7-tetrahydro-1-benzothiophene-3-carboxylate

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Technology Process of ethyl 2-{[(phenylcarbonyl)carbamothioyl]amino}-4,5,6,7-tetrahydro-1-benzothiophene-3-carboxylate

There total 1 articles about ethyl 2-{[(phenylcarbonyl)carbamothioyl]amino}-4,5,6,7-tetrahydro-1-benzothiophene-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 4506-71-2
ethyl 2-amino-4,5,6,7-tetrahydrobenzo[b]thiophene-3-carboxylate

: 532-55-8
Benzoyl isothiocyanate

: 53162-41-7
ethyl 2-(3-benzoylthioureido)-4,5,6,7-tetrahydrobenzo[b]thiophene-3-carboxylate

Guidance literature:: In acetone; for 3h; Reflux;
DOI:10.1002/jhet.1554

Reference yield: 95.0%

: 53162-41-7
ethyl 2-(3-benzoylthioureido)-4,5,6,7-tetrahydrobenzo[b]thiophene-3-carboxylate

: 321971-43-1
ethyl (4-oxo-2-mercapto-4,5,6,7-terahydrobenzo[b]thieno[2,3-d]pyrimidin-3(4H)-yl)-(phenyl)carboxylate

Guidance literature:: With sodium ethanolate; In ethanol; for 3h; Reflux;
DOI:10.1002/jhet.1554

Reference yield: 93.0%

: 53162-41-7
ethyl 2-(3-benzoylthioureido)-4,5,6,7-tetrahydrobenzo[b]thiophene-3-carboxylate

: 100-39-0
benzyl bromide

: 324036-21-7
2-(benzylsulfanyl)-5,6,7,8-tetrahydrobenzo[4,5]thieno[2,3-d]-pyrimidin-4(3H)-one

Guidance literature:: ethyl 2-(3-benzoylthioureido)-4,5,6,7-tetrahydrobenzo[b]thiophene-3-carboxylate; With sodium hydroxide; In ethanol; for 2h; Reflux;

benzyl bromide; In ethanol; at 20 ℃; for 2h;
DOI:10.1021/jo4010876