Technology Process of C25H40N2O3
There total 8 articles about C25H40N2O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
phosgene; (2E,4E)-N-methyIdodeca-2,4-dien-1-amine hydrochloride;
With
N-ethyl-N,N-diisopropylamine;
In
dichloromethane; toluene;
at 0 - 20 ℃;
N-methylhomoveratrylamine;
In
dichloromethane; toluene;
at 20 ℃;
for 15h;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: diisobutylaluminium hydride / n-heptane; hexane / 0.75 h / -70 °C / Inert atmosphere
2.1: diphenylphosphoranyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / toluene
3.1: lithium aluminium tetrahydride / diethyl ether / 2 h / 0 - 20 °C / Inert atmosphere; Cooling with ice
4.1: triethylamine / 15 h / 20 °C
5.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 20 °C / Inert atmosphere
5.2: 4 h
6.1: hydrogenchloride / 1,4-dioxane; diethyl ether / 1 h / 20 °C
7.1: N-ethyl-N,N-diisopropylamine / dichloromethane; toluene / 0 - 20 °C
7.2: 15 h / 20 °C
With
hydrogenchloride; lithium aluminium tetrahydride; diphenylphosphoranyl azide; sodium hydride; diisobutylaluminium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; N-ethyl-N,N-diisopropylamine;
In
1,4-dioxane; diethyl ether; hexane; n-heptane; dichloromethane; N,N-dimethyl-formamide; toluene; mineral oil;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: hydrogenchloride / 1,4-dioxane; diethyl ether / 1 h / 20 °C
2.1: N-ethyl-N,N-diisopropylamine / dichloromethane; toluene / 0 - 20 °C
2.2: 15 h / 20 °C
With
hydrogenchloride; N-ethyl-N,N-diisopropylamine;
In
1,4-dioxane; diethyl ether; dichloromethane; toluene;
