1,5-bis((S)-5,5-dimethyl-2-oxo-4-phenyloxazolidin-3-yl)-2-isopropyl-3-methylpentane-1,5-dione

Base Information

• Chemical Name: 1,5-bis((S)-5,5-dimethyl-2-oxo-4-phenyloxazolidin-3-yl)-2-isopropyl-3-methylpentane-1,5-dione
• CAS No.: 1359091-85-2
• Molecular Formula: C₃₁H₃₈N₂O₆
• Molecular Weight: 534.653

Synonyms:1,5-bis((S)-5,5-dimethyl-2-oxo-4-phenyloxazolidin-3-yl)-2-isopropyl-3-methylpentane-1,5-dione

Chemical Property of 1,5-bis((S)-5,5-dimethyl-2-oxo-4-phenyloxazolidin-3-yl)-2-isopropyl-3-methylpentane-1,5-dione

Chemical Property:

Purity/Quality:

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Technology Process of 1,5-bis((S)-5,5-dimethyl-2-oxo-4-phenyloxazolidin-3-yl)-2-isopropyl-3-methylpentane-1,5-dione

There total 1 articles about 1,5-bis((S)-5,5-dimethyl-2-oxo-4-phenyloxazolidin-3-yl)-2-isopropyl-3-methylpentane-1,5-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C15H17NO3 + methylmagnesium bromide (75-16-1) → 1,5-bis((S)-5,5-dimethyl-2-oxo-4-phenyloxazolidin-3-yl)-2-isopropyl-3-methylpentane-1,5-dione (1359091-90-9) + 1,5-bis((S)-5,5-dimethyl-2-oxo-4-phenyloxazolidin-3-yl)-2-isopropyl-3-methylpentane-1,5-dione (1359091-85-2)

Guidance literature:

methylmagnesium bromide; With copper(I) bromide dimethylsulfide complex; dimethylsulfide; In tetrahydrofuran; at -40 - -15 ℃; Inert atmosphere;

C₁₅H₁₇NO₃; In tetrahydrofuran;

With ammonium hydroxide; water; In tetrahydrofuran; at 20 ℃; for 0.5h; optical yield given as %de; diastereoselective reaction;

DOI:10.1016/j.tet.2011.12.046

upstream raw materials:

methylmagnesium bromide

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