{OsI(C₆H₆)(P(CH(CH₃)2)3)(NHC(C₆H₅)2)}⁽¹⁺⁾*PF₆^(1-)={OsI(C₆H₆)(P(CH(CH₃)2)3)(NHC(C₆H₅)2)}PF₆

Base Information

• Chemical Name: {OsI(C₆H₆)(P(CH(CH₃)2)3)(NHC(C₆H₅)2)}⁽¹⁺⁾*PF₆^(1-)={OsI(C₆H₆)(P(CH(CH₃)2)3)(NHC(C₆H₅)2)}PF₆
• CAS No.: 135455-16-2
• Molecular Formula: C₂₈H₃₈INOsP*F₆P
• Molecular Weight: 881.659

Synonyms:{OsI(C₆H₆)(P(CH(CH₃)2)3)(NHC(C₆H₅)2)}⁽¹⁺⁾*PF₆^(1-)={OsI(C₆H₆)(P(CH(CH₃)2)3)(NHC(C₆H₅)2)}PF₆

Chemical Property of {OsI(C₆H₆)(P(CH(CH₃)2)3)(NHC(C₆H₅)2)}⁽¹⁺⁾*PF₆^(1-)={OsI(C₆H₆)(P(CH(CH₃)2)3)(NHC(C₆H₅)2)}PF₆

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Technology Process of {OsI(C₆H₆)(P(CH(CH₃)2)3)(NHC(C₆H₅)2)}⁽¹⁺⁾*PF₆^(1-)={OsI(C₆H₆)(P(CH(CH₃)2)3)(NHC(C₆H₅)2)}PF₆

There total 1 articles about {OsI(C₆H₆)(P(CH(CH₃)2)3)(NHC(C₆H₅)2)}⁽¹⁺⁾*PF₆^(1-)={OsI(C₆H₆)(P(CH(CH₃)2)3)(NHC(C₆H₅)2)}PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

Benzophenone imine (1013-88-3) + silver(I) hexafluorophosphate (26042-63-7) + (η6-C6H6)OsI2(P-i-Pr3) (97477-25-3) → {OsI(C6H6)(P(CH(CH3)2)3)(NHC(C6H5)2)}(1+)*PF6(1-)={OsI(C6H6)(P(CH(CH3)2)3)(NHC(C6H5)2)}PF6 (135455-16-2)

Guidance literature:

In dichloromethane; under Ar, addn. of imine in CH2Cl2 to a solid mixture of AgPF6 and Os-compd. at -78°C, warmed to room temp., stirred for 10 min; filtered, evapd. in vac., addn. of ether, filtered, washed with ether, dried in vac.; elem. anal.;

Reference yield: 92.0%

{OsI(C6H6)(P(CH(CH3)2)3)(NHC(C6H5)2)}(1+)*PF6(1-)={OsI(C6H6)(P(CH(CH3)2)3)(NHC(C6H5)2)}PF6 (135455-16-2) → {Os(C6H6)(P(CH(CH3)2)3)(NC(C6H5)2)}(1+)*PF6(1-)={Os(C6H6)(P(CH(CH3)2)3)(NC(C6H5)2)}PF6 (135455-18-4)

Guidance literature:

With N(C₂H₅)3; In dichloromethane; byproducts: HI; under Ar, stirred for 15 min at room temp.; removal of solvent in vac., dissolved in CH2Cl2, chromy. (Al2O3, CH2Cl2), evapn. to dryness, recrystn. (CH2Cl2/ether);

upstream raw materials:

Benzophenone imine

silver(I) hexafluorophosphate

(η6-C6H6)OsI2(P-i-Pr3)

Downstream raw materials:

{Os(C₆H₆)(P(CH(CH₃)2)3)(NC(C₆H₅)2)}⁽¹⁺⁾*PF₆^(1-)={Os(C₆H₆)(P(CH(CH₃)2)3)(NC(C₆H₅)2)}PF₆

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