1-carbonyl>amino>-2-methyl-2-cyclohexene

Base Information

Chemical Name:1-carbonyl>amino>-2-methyl-2-cyclohexene
CAS No.:132646-17-4
Molecular Formula:C₂₀H₂₇NO₂
Molecular Weight:313.44
Hs Code.:

1-<N-<<(trans-2-phenylcyclohexyl)oxy>carbonyl>amino>-2-methyl-2-cyclohexene

Synonyms:1-carbonyl>amino>-2-methyl-2-cyclohexene

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Chemical Property of 1-carbonyl>amino>-2-methyl-2-cyclohexene

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Technology Process of 1-carbonyl>amino>-2-methyl-2-cyclohexene

There total 4 articles about 1-carbonyl>amino>-2-methyl-2-cyclohexene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₃H₃₅NO₃SSi

: 132646-17-4
1-carbonyl>amino>-2-methyl-2-cyclohexene

Guidance literature:: With lithium hydroxide; water; In tetrahydrofuran; methanol; for 3h; Yield given; Ambient temperature;
DOI:10.1021/ja00009a045

Reference yield:

: 129966-10-5
(S)-trans-2-phenylcyclohexyl carbamate

: 132646-17-4
1-carbonyl>amino>-2-methyl-2-cyclohexene

Guidance literature:: Multi-step reaction with 4 steps

1: SOCl₂, pyridine / benzene / 14.25 h / Ambient temperature

2: SnCl₄ / CH₂Cl₂ / 0.33 h / -78 °C

3: 1,2-dichloro-ethane / 1.) RT, 90 min, 2.) 50 deg C, 90 min, 3.) reflux, overnight

4: LiOH, H₂O / tetrahydrofuran; methanol / 3 h / Ambient temperature

With pyridine; lithium hydroxide; thionyl chloride; water; tin(IV) chloride; In tetrahydrofuran; methanol; dichloromethane; 1,2-dichloro-ethane; benzene;
DOI:10.1021/ja00009a045

Reference yield:

: 107575-41-7,130060-02-5
(S)-trans-2-phenylcyclohexyl N-sulfinylcarbamate

: 132646-17-4
1-carbonyl>amino>-2-methyl-2-cyclohexene

Guidance literature:: Multi-step reaction with 3 steps

1: SnCl₄ / CH₂Cl₂ / 0.33 h / -78 °C

2: 1,2-dichloro-ethane / 1.) RT, 90 min, 2.) 50 deg C, 90 min, 3.) reflux, overnight

3: LiOH, H₂O / tetrahydrofuran; methanol / 3 h / Ambient temperature

With lithium hydroxide; water; tin(IV) chloride; In tetrahydrofuran; methanol; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1021/ja00009a045