C₅₅H₆₀N₁₂O₉S₆Si

Base Information

Chemical Name:C₅₅H₆₀N₁₂O₉S₆Si
CAS No.:924288-54-0
Molecular Formula:C₅₅H₆₀N₁₂O₉S₆Si
Molecular Weight:1253.64
Hs Code.:

C<sub>55</sub>H<sub>60</sub>N<sub>12</sub>O<sub>9</sub>S<sub>6</sub>Si

Synonyms:C₅₅H₆₀N₁₂O₉S₆Si

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Chemical Property of C₅₅H₆₀N₁₂O₉S₆Si

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Technology Process of C₅₅H₆₀N₁₂O₉S₆Si

There total 28 articles about C₅₅H₆₀N₁₂O₉S₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 924288-49-3
C₆₁H₇₂N₁₂O₁₂S₆Si

: 924288-54-0
C₅₅H₆₀N₁₂O₉S₆Si

Guidance literature:: C₆₁H₇₂N₁₂O₁₂S₆Si; With trimethyltin(IV) hydroxide; In 1,2-dichloro-ethane; at 60 ℃; for 16h;

With trifluoroacetic acid; In dichloromethane; at 25 ℃; for 1h;

With pentafluorophenyl diphenyl-phosphinate; N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide; for 24h;
DOI:10.1002/anie.200602798

Reference yield:

: 2-tert-butoxycarbonylamino-3-(tert-butyl-dimethyl-silanyloxy)-3-phenyl-propionic acid

: 924288-54-0
C₅₅H₆₀N₁₂O₉S₆Si

Guidance literature:: Multi-step reaction with 9 steps

1.1: trifluoroacetic acid / H₂O / 1 h / 25 °C

1.2: 85 percent / HATU; i-Pr₂NEt / CH₂Cl₂ / 3 h / 25 °C

2.1: 82 percent / imidazole / dimethylformamide / 16 h / 25 °C

3.1: 80 percent / Lawesson reagent / benzene / 16 h / Heating

4.1: 92 percent / HF*pyridine; pyridine / tetrahydrofuran / 2 h / 25 °C

5.1: N,N-diethylaminosulfur trifluoride / CH₂Cl₂ / 1 h / -78 °C

6.1: BrCCl₃; 1,8-diazabicyclo[5.4.0]undec-7-ene / CH₂Cl₂ / 1 h / 0 °C

7.1: trifluoroacetic acid / CH₂Cl₂ / 1 h / 25 °C

8.1: HATU; i-Pr₂NEt / CH₂Cl₂ / 24 h / 25 °C

With Lawessons reagent; pyridine; 1H-imidazole; Bromotrichloromethane; diethylamino-sulfur trifluoride; pyridine hydrogenfluoride; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; benzene;
DOI:10.1002/anie.200602798

Reference yield:

: 924288-30-2
4-{4-[3-amino-3,6-bis-(4-methoxycarbonyl-thiazol-2-yl)-2,3,4,5-tetrahydro-pyridin-2-yl]-thiazol-2-yl}-2,2-dimethyl-oxazolidine-3-carboxylic acid tert-butyl ester

: 924288-54-0
C₅₅H₆₀N₁₂O₉S₆Si

Guidance literature:: Multi-step reaction with 10 steps

1.1: 50 percent / 1,8-diazabicyclo[5.4.0]undec-7-ene / ethyl acetate / 5 h / Heating

2.1: trifluoroacetic acid / H₂O / 1 h / 25 °C

2.2: 85 percent / HATU; i-Pr₂NEt / CH₂Cl₂ / 3 h / 25 °C

3.1: 82 percent / imidazole / dimethylformamide / 16 h / 25 °C

4.1: 80 percent / Lawesson reagent / benzene / 16 h / Heating

5.1: 92 percent / HF*pyridine; pyridine / tetrahydrofuran / 2 h / 25 °C

6.1: N,N-diethylaminosulfur trifluoride / CH₂Cl₂ / 1 h / -78 °C

7.1: BrCCl₃; 1,8-diazabicyclo[5.4.0]undec-7-ene / CH₂Cl₂ / 1 h / 0 °C

8.1: trifluoroacetic acid / CH₂Cl₂ / 1 h / 25 °C

9.1: HATU; i-Pr₂NEt / CH₂Cl₂ / 24 h / 25 °C

With Lawessons reagent; pyridine; 1H-imidazole; Bromotrichloromethane; diethylamino-sulfur trifluoride; pyridine hydrogenfluoride; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In tetrahydrofuran; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; benzene;
DOI:10.1002/anie.200602798