2-nitro-<α-D>-styrene

Base Information

Chemical Name:2-nitro-<α-D>-styrene
CAS No.:89650-54-4
Molecular Formula:C₈H₇NO₂
Molecular Weight:150.141
Hs Code.:

Synonyms:2-nitro-<α-D>-styrene

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Chemical Property of 2-nitro-<α-D>-styrene

Chemical Property:

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Technology Process of 2-nitro-<α-D>-styrene

There total 6 articles about 2-nitro-<α-D>-styrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 50344-83-7
2-nitrobenzaldehyde-α-d₁

: 1779-49-3
Methyltriphenylphosphonium bromide

: 89650-54-4
2-nitro-<α-D>-styrene

Guidance literature:: Methyltriphenylphosphonium bromide; With n-butyllithium; In tetrahydrofuran; cyclohexane; at 0 - 20 ℃; for 1h; Inert atmosphere;

2-nitrobenzaldehyde-α-d₁; In tetrahydrofuran; cyclohexane; at 65 ℃; for 5h;
DOI:10.1002/anie.201402661

Reference yield:

: 3592-47-0
Benzaldehyde-d

: 89650-54-4
2-nitro-<α-D>-styrene

Guidance literature:: Multi-step reaction with 2 steps

1: BuLi, Ph₃P / tetrahydrofuran

2: HNO₃ / acetic anhydride

With n-butyllithium; nitric acid; triphenylphosphine; In tetrahydrofuran; acetic anhydride;
DOI:10.1002/oms.1210181214

Reference yield:

: 606-27-9
methyl 2-nitrobenzoate

: 89650-54-4
2-nitro-<α-D>-styrene

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium aluminium deuteride / diethyl ether / 0 - 20 °C / Inert atmosphere; Schlenk technique

2.1: Dess-Martin periodane / dichloromethane / 2 h / 20 °C

3.1: n-butyllithium / tetrahydrofuran; cyclohexane / 1 h / 0 - 20 °C / Inert atmosphere

3.2: 5 h / 65 °C

With n-butyllithium; lithium aluminium deuteride; Dess-Martin periodane; In tetrahydrofuran; diethyl ether; dichloromethane; cyclohexane;
DOI:10.1002/anie.201402661