3,6,7-tri-O-acetyl-5-(N-benzoxycarbonylamino)-5-deoxy-1,2-O-isopropylidene-β-L-glycero-L-ido-heptofuranose

Base Information

Chemical Name:3,6,7-tri-O-acetyl-5-(N-benzoxycarbonylamino)-5-deoxy-1,2-O-isopropylidene-β-L-glycero-L-ido-heptofuranose
CAS No.:870078-05-0
Molecular Formula:C₂₄H₃₁NO₁₁
Molecular Weight:509.51
Hs Code.:

Synonyms:3,6,7-tri-O-acetyl-5-(N-benzoxycarbonylamino)-5-deoxy-1,2-O-isopropylidene-β-L-glycero-L-ido-heptofuranose

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Chemical Property of 3,6,7-tri-O-acetyl-5-(N-benzoxycarbonylamino)-5-deoxy-1,2-O-isopropylidene-β-L-glycero-L-ido-heptofuranose

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Technology Process of 3,6,7-tri-O-acetyl-5-(N-benzoxycarbonylamino)-5-deoxy-1,2-O-isopropylidene-β-L-glycero-L-ido-heptofuranose

There total 7 articles about 3,6,7-tri-O-acetyl-5-(N-benzoxycarbonylamino)-5-deoxy-1,2-O-isopropylidene-β-L-glycero-L-ido-heptofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 870078-04-9
5-(N-benzoxycarbonyl)amino-3,6,7-trihydroxy-5-deoxy-1,2-O-isopropylidene-β-L-glycero-L-ido-hepto-1,4-furanose

: 108-24-7
acetic anhydride

: 870078-05-0
3,6,7-tri-O-acetyl-5-(N-benzoxycarbonylamino)-5-deoxy-1,2-O-isopropylidene-β-L-glycero-L-ido-heptofuranose

Guidance literature:: With pyridine; at 25 ℃; for 6h;
DOI:10.1039/b509216g

Reference yield:

: (2R,3S)-3-Benzylamino-3-((3aR,5R,6S,6aR)-6-benzyloxy-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-5-yl)-propane-1,2-diol

: 870078-05-0
3,6,7-tri-O-acetyl-5-(N-benzoxycarbonylamino)-5-deoxy-1,2-O-isopropylidene-β-L-glycero-L-ido-heptofuranose

Guidance literature:: Multi-step reaction with 3 steps

1: HCOONH₄ / Pd/C / ethanol / 2 h / Heating

2: 0.76 g / aq. NaHCO₃ / ethanol / 3.5 h / 25 °C

3: 86 percent / pyridine / 6 h / 25 °C

With pyridine; ammonium formate; sodium hydrogencarbonate; palladium on activated charcoal; In ethanol;
DOI:10.1039/b509216g

Reference yield:

: 870078-01-6
ethyl 3-O-benzyl-5-(N-benzyl)amino-1,2-O-isopropylidene-β-L-glycero-L-ido-heptofuranuronate

: 870078-05-0
3,6,7-tri-O-acetyl-5-(N-benzoxycarbonylamino)-5-deoxy-1,2-O-isopropylidene-β-L-glycero-L-ido-heptofuranose

Guidance literature:: Multi-step reaction with 4 steps

1: LiAlH₄ / tetrahydrofuran / 2 h / 25 °C

2: HCOONH₄ / Pd/C / ethanol / 2 h / Heating

3: 0.76 g / aq. NaHCO₃ / ethanol / 3.5 h / 25 °C

4: 86 percent / pyridine / 6 h / 25 °C

With pyridine; lithium aluminium tetrahydride; ammonium formate; sodium hydrogencarbonate; palladium on activated charcoal; In tetrahydrofuran; ethanol;
DOI:10.1039/b509216g