ethyl 3-O-benzyl-5-(N-benzyl)amino-1,2-O-isopropylidene-β-L-glycero-L-ido-heptofuranuronate

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Chemical Name:ethyl 3-O-benzyl-5-(N-benzyl)amino-1,2-O-isopropylidene-β-L-glycero-L-ido-heptofuranuronate
CAS No.:870078-01-6
Molecular Formula:C₂₆H₃₃NO₇
Molecular Weight:471.551
Hs Code.:

Synonyms:ethyl 3-O-benzyl-5-(N-benzyl)amino-1,2-O-isopropylidene-β-L-glycero-L-ido-heptofuranuronate

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Chemical Property of ethyl 3-O-benzyl-5-(N-benzyl)amino-1,2-O-isopropylidene-β-L-glycero-L-ido-heptofuranuronate

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Technology Process of ethyl 3-O-benzyl-5-(N-benzyl)amino-1,2-O-isopropylidene-β-L-glycero-L-ido-heptofuranuronate

There total 3 articles about ethyl 3-O-benzyl-5-(N-benzyl)amino-1,2-O-isopropylidene-β-L-glycero-L-ido-heptofuranuronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 870078-00-5
ethyl 3-O-benzyl-5,6-N-benzyl-(E)-aziridine-1,2-O-isopropylidenehept-5,6-dideoxy-β-L-ido-heptofuranuronate

: 870078-01-6
ethyl 3-O-benzyl-5-(N-benzyl)amino-1,2-O-isopropylidene-β-L-glycero-L-ido-heptofuranuronate

Guidance literature:: With trifluoroacetic acid; In acetone; at 25 ℃; for 24h;
DOI:10.1039/b509216g

Reference yield:

: 57972-96-0,71536-59-9
(E)-3-((3aR,5R,6S,6aR)-6-Benzyloxy-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-5-yl)-2-bromo-acrylic acid ethyl ester

: 870078-01-6
ethyl 3-O-benzyl-5-(N-benzyl)amino-1,2-O-isopropylidene-β-L-glycero-L-ido-heptofuranuronate

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / benzene / 6 h / 25 °C

2: 82 percent / aq. TFA / acetone / 24 h / 25 °C

With trifluoroacetic acid; In acetone; benzene;
DOI:10.1039/b509216g

Reference yield:

: 23558-05-6
3-O-benzyl-1,2-O-isopropylidene-1,5-D-xylo-dialdofuranose

: 870078-01-6
ethyl 3-O-benzyl-5-(N-benzyl)amino-1,2-O-isopropylidene-β-L-glycero-L-ido-heptofuranuronate

Guidance literature:: Multi-step reaction with 3 steps

1: 77 percent / CH₂Cl₂ / 12 h / 25 °C

2: 70 percent / benzene / 6 h / 25 °C

3: 82 percent / aq. TFA / acetone / 24 h / 25 °C

With trifluoroacetic acid; In dichloromethane; acetone; benzene; 1: Wittig reaction;
DOI:10.1039/b509216g