methyl 2,12-7-phenyl-5,6,7,8-tetrahydro-1,13-diazadibenzanthracene-14-carboxylate

Base Information

Chemical Name:methyl 2,12-7-phenyl-5,6,7,8-tetrahydro-1,13-diazadibenzanthracene-14-carboxylate
CAS No.:130883-20-4
Molecular Formula:C₂₈H₂₀Br₂N₂O₂
Molecular Weight:576.287
Hs Code.:

methyl 2,12-7-phenyl-5,6,7,8-tetrahydro-1,13-diazadibenz<a,j>anthracene-14-carboxylate

Synonyms:methyl 2,12-7-phenyl-5,6,7,8-tetrahydro-1,13-diazadibenzanthracene-14-carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 2,12-7-phenyl-5,6,7,8-tetrahydro-1,13-diazadibenzanthracene-14-carboxylate

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Technology Process of methyl 2,12-7-phenyl-5,6,7,8-tetrahydro-1,13-diazadibenzanthracene-14-carboxylate

There total 1 articles about methyl 2,12-7-phenyl-5,6,7,8-tetrahydro-1,13-diazadibenzanthracene-14-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 113493-51-9
methyl(dimethylphosphinyl)acetate

: 130883-19-1
2,12-Dibromo-7-phenyl-5,7,8,9-tetrahydro-6H-14-oxa-1,13-diaza-dibenzo[a,j]anthracene

: 130883-20-4
methyl 2,12-7-phenyl-5,6,7,8-tetrahydro-1,13-diazadibenzanthracene-14-carboxylate

Guidance literature:: Yield given. Multistep reaction;
DOI:10.1021/ja00001a027

Reference yield: 73.0%

: 92103-92-9
9-phenanthrenylmagnesium bromide

: 130883-20-4
methyl 2,12-7-phenyl-5,6,7,8-tetrahydro-1,13-diazadibenzanthracene-14-carboxylate

: 129363-22-0
methyl 2,12-bis(9-anthracenyl)-7-phenyl-5,6,8,9-tetrahydro-1,13-diazadibenzanthracene-14-carboxylate

Guidance literature:: DOI:10.1021/jo00303a006

Reference yield:

: 130883-20-4
methyl 2,12-7-phenyl-5,6,7,8-tetrahydro-1,13-diazadibenzanthracene-14-carboxylate

: 129337-84-4
2,12-bis(9-anthracenyl)-7-phenyl-5,6,8,9-tetrahydro-1,13-diazadibenzanthracene-14-carboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) magnesium, 1,2-dibromoethane, iodine, 2.) Ni(acac)2 / 1.) Et₂O, 50 deg C, 1 h, 2.) a) benzene, 0 deg C, 1 h, b) reflux, 24 h

2: 50 percent / boron trichloride / CH₂Cl₂; hexane / Heating

With bis(acetylacetonate)nickel(II); iodine; boron trichloride; magnesium; ethylene dibromide; In hexane; dichloromethane;
DOI:10.1021/ja00001a027