Methanesulfonic acid (S)-1-(3-benzyloxycarbonylamino-propyl)-pentadecyl ester

Base Information

Chemical Name:Methanesulfonic acid (S)-1-(3-benzyloxycarbonylamino-propyl)-pentadecyl ester
CAS No.:205322-71-0
Molecular Formula:C₂₇H₄₇NO₅S
Molecular Weight:497.74
Hs Code.:

Synonyms:Methanesulfonic acid (S)-1-(3-benzyloxycarbonylamino-propyl)-pentadecyl ester

Suppliers and Price of Methanesulfonic acid (S)-1-(3-benzyloxycarbonylamino-propyl)-pentadecyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Methanesulfonic acid (S)-1-(3-benzyloxycarbonylamino-propyl)-pentadecyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Methanesulfonic acid (S)-1-(3-benzyloxycarbonylamino-propyl)-pentadecyl ester

There total 5 articles about Methanesulfonic acid (S)-1-(3-benzyloxycarbonylamino-propyl)-pentadecyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 124-63-0
methanesulfonyl chloride

: 205322-57-2
(S)-N-benzyloxycarbonyl-1-aminopropylpentadecan-1-ol

: 205322-71-0
Methanesulfonic acid (S)-1-(3-benzyloxycarbonylamino-propyl)-pentadecyl ester

Guidance literature:: With dmap; In pyridine; at 0 ℃; for 2h;
DOI:10.3987/COM-97-S26

Reference yield:

: 205322-54-9
2-((R)-4,5-Dihydroxy-pentyl)-isoindole-1,3-dione

: 205322-71-0
Methanesulfonic acid (S)-1-(3-benzyloxycarbonylamino-propyl)-pentadecyl ester

Guidance literature:: Multi-step reaction with 4 steps

2: 75 percent / CuI / tetrahydrofuran / 2 h / 0 °C

3: 1.) 100percent hydrazine hydrate, conc.HCl; 2.) 2N NaOH / 1.) ethanol, reflux, 3.5 h, r.t.; 2.) 0 deg C, 2 h, r.t.

4: 87 percent / DMAP / pyridine / 2 h / 0 °C

With hydrogenchloride; dmap; sodium hydroxide; copper(l) iodide; hydrazine hydrate; In tetrahydrofuran; pyridine;
DOI:10.3987/COM-97-S26

Reference yield:

: 205322-56-1
2-((S)-4-Hydroxy-octadecyl)-isoindole-1,3-dione

: 205322-71-0
Methanesulfonic acid (S)-1-(3-benzyloxycarbonylamino-propyl)-pentadecyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) 100percent hydrazine hydrate, conc.HCl; 2.) 2N NaOH / 1.) ethanol, reflux, 3.5 h, r.t.; 2.) 0 deg C, 2 h, r.t.

2: 87 percent / DMAP / pyridine / 2 h / 0 °C

With hydrogenchloride; dmap; sodium hydroxide; hydrazine hydrate; In pyridine;
DOI:10.3987/COM-97-S26