(1S,2S)-N-((4-ethoxycarbonyl)methoxybenzenesulfonyl)-1,2-diphenylethylenediamine

Base Information

Chemical Name:(1S,2S)-N-((4-ethoxycarbonyl)methoxybenzenesulfonyl)-1,2-diphenylethylenediamine
CAS No.:863483-24-3
Molecular Formula:C₂₄H₂₆N₂O₅S
Molecular Weight:454.547
Hs Code.:

Synonyms:(1S,2S)-N-((4-ethoxycarbonyl)methoxybenzenesulfonyl)-1,2-diphenylethylenediamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,2S)-N-((4-ethoxycarbonyl)methoxybenzenesulfonyl)-1,2-diphenylethylenediamine

Chemical Property:

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Technology Process of (1S,2S)-N-((4-ethoxycarbonyl)methoxybenzenesulfonyl)-1,2-diphenylethylenediamine

There total 3 articles about (1S,2S)-N-((4-ethoxycarbonyl)methoxybenzenesulfonyl)-1,2-diphenylethylenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 29841-69-8
(S,S)-1,2-diphenyl-1,2-diaminoethane

: 36685-84-4
(4-chlorosulfonyl-phenoxy)acetic acid ethyl ester

: 863483-24-3
(1S,2S)-N-((4-ethoxycarbonyl)methoxybenzenesulfonyl)-1,2-diphenylethylenediamine

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 4h;
DOI:10.1039/b505943g

Reference yield:

: sodium 4-((ethoxycarbonyl)methoxy)benzenesulfonate

: 863483-24-3
(1S,2S)-N-((4-ethoxycarbonyl)methoxybenzenesulfonyl)-1,2-diphenylethylenediamine

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / SOCl₂ / dimethylformamide / 2 h / 60 °C

2: 55 percent / Et₃N / CH₂Cl₂ / 4 h / 20 °C

With thionyl chloride; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/b505943g

Reference yield:

: 825-90-1
sodium p-hydroxybenzenesulfonate

: 863483-24-3
(1S,2S)-N-((4-ethoxycarbonyl)methoxybenzenesulfonyl)-1,2-diphenylethylenediamine

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / K₂CO₃; dibenzo-18-crown-6 / acetone / 48 h / Heating

2: 67 percent / SOCl₂ / dimethylformamide / 2 h / 60 °C

3: 55 percent / Et₃N / CH₂Cl₂ / 4 h / 20 °C

With dibenzo-18-crown-6; thionyl chloride; potassium carbonate; triethylamine; In dichloromethane; N,N-dimethyl-formamide; acetone;
DOI:10.1039/b505943g