(S)-2-(1-chloro-2-cyclohexylethyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Base Information

Chemical Name:(S)-2-(1-chloro-2-cyclohexylethyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
CAS No.:1360649-37-1
Molecular Formula:C₁₄H₂₆BClO₂
Molecular Weight:272.623
Hs Code.:

Synonyms:(S)-2-(1-chloro-2-cyclohexylethyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-2-(1-chloro-2-cyclohexylethyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Technology Process of (S)-2-(1-chloro-2-cyclohexylethyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

There total 9 articles about (S)-2-(1-chloro-2-cyclohexylethyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1360649-11-1
2-(1-chloro-2-cyclohexylvinyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 1360649-37-1
(S)-2-(1-chloro-2-cyclohexylethyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 167692-95-7
2-cyclohexyl-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)ethane

Guidance literature:: With C₅₂H₄₇FeIrN₂OP⁽¹⁺⁾*C₃₂H₁₂BF₂₄^(1-); hydrogen; In dichloromethane; at 50 ℃; for 18h; under 22502.3 Torr; enantioselective reaction; Inert atmosphere;
DOI:10.1055/s-0033-1338512

Reference yield: 85.0%

: 1360649-11-1
2-(1-chloro-2-cyclohexylvinyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 1360649-37-1
(S)-2-(1-chloro-2-cyclohexylethyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: With (η-1,5-cyclooctadiene) {[4(R),5(R)]-1-benzoyl-2-[(S)-2-diphenylphosphinoferrocenyl]-4,5-diphenyl-4,5-dihydro-1-imidazole} iridium(I) tetrakis[3,5-bis(trifluoromethyl)phenyl]borate; hydrogen; In dichloromethane; at 50 ℃; for 18h; under 22502.3 Torr; optical yield given as %ee; enantioselective reaction;
DOI:10.1002/anie.201106262

Reference yield:

: 1360649-11-1
2-(1-chloro-2-cyclohexylvinyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 1360649-37-1
(S)-2-(1-chloro-2-cyclohexylethyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: (R)-2-(1-chloro-2-cyclohexylethyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: With (η-1,5-cyclooctadiene) {[4(R),5(R)]-1-benzoyl-2-[(S)-2-diphenylphosphinoferrocenyl]-4,5-diphenyl-4,5-dihydro-1-imidazole} iridium(I) tetrakis[3,5-bis(trifluoromethyl)phenyl]borate; hydrogen; In dichloromethane; at 50 ℃; for 18h; under 22502.3 Torr; optical yield given as %ee; enantioselective reaction;
DOI:10.1002/anie.201106262