{(3aS,4R,7R)-2-Benzoyl-1-benzyl-4-[(E)-3-(tert-butyl-dimethyl-silanyloxy)-propenyl]-7-methyl-3-oxo-6-trimethylsilanylmethyl-1,2,3,4,7,7a-hexahydro-isoindol-3a-yl}-oxo-ethanethial

Base Information

Chemical Name:{(3aS,4R,7R)-2-Benzoyl-1-benzyl-4-[(E)-3-(tert-butyl-dimethyl-silanyloxy)-propenyl]-7-methyl-3-oxo-6-trimethylsilanylmethyl-1,2,3,4,7,7a-hexahydro-isoindol-3a-yl}-oxo-ethanethial
CAS No.:90741-77-8
Molecular Formula:C₃₈H₅₁NO₄SSi₂
Molecular Weight:674.064
Hs Code.:

{(3aS,4R,7R)-2-Benzoyl-1-benzyl-4-[(E)-3-(tert-butyl-dimethyl-silanyloxy)-propenyl]-7-methyl-3-oxo-6-trimethylsilanylmethyl-1,2,3,4,7,7a-hexahydro-isoindol-3a-yl}-oxo-ethanethial

Synonyms:{(3aS,4R,7R)-2-Benzoyl-1-benzyl-4-[(E)-3-(tert-butyl-dimethyl-silanyloxy)-propenyl]-7-methyl-3-oxo-6-trimethylsilanylmethyl-1,2,3,4,7,7a-hexahydro-isoindol-3a-yl}-oxo-ethanethial

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Chemical Property of {(3aS,4R,7R)-2-Benzoyl-1-benzyl-4-[(E)-3-(tert-butyl-dimethyl-silanyloxy)-propenyl]-7-methyl-3-oxo-6-trimethylsilanylmethyl-1,2,3,4,7,7a-hexahydro-isoindol-3a-yl}-oxo-ethanethial

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Technology Process of {(3aS,4R,7R)-2-Benzoyl-1-benzyl-4-[(E)-3-(tert-butyl-dimethyl-silanyloxy)-propenyl]-7-methyl-3-oxo-6-trimethylsilanylmethyl-1,2,3,4,7,7a-hexahydro-isoindol-3a-yl}-oxo-ethanethial

There total 2 articles about {(3aS,4R,7R)-2-Benzoyl-1-benzyl-4-[(E)-3-(tert-butyl-dimethyl-silanyloxy)-propenyl]-7-methyl-3-oxo-6-trimethylsilanylmethyl-1,2,3,4,7,7a-hexahydro-isoindol-3a-yl}-oxo-ethanethial which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 90741-75-6
(4R,7R,7aS)-2-Benzoyl-3-benzyl-7-[(E)-3-(tert-butyl-dimethyl-silanyloxy)-propenyl]-7a-(2-chloro-acetyl)-4-methyl-5-trimethylsilanylmethyl-2,3,3a,4,7,7a-hexahydro-isoindol-1-one

: 90741-77-8
{(3aS,4R,7R)-2-Benzoyl-1-benzyl-4-[(E)-3-(tert-butyl-dimethyl-silanyloxy)-propenyl]-7-methyl-3-oxo-6-trimethylsilanylmethyl-1,2,3,4,7,7a-hexahydro-isoindol-3a-yl}-oxo-ethanethial

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / K₂CO₃ / tetrahydrofuran

2: Irradiation

With potassium carbonate; In tetrahydrofuran;
DOI:10.1021/ja00328a053