N-[2-(3,4-bis-benzyloxy-phenyl)-ethyl]-succinamic-L-phenylalanyl-L-phenylalanine

Base Information

Chemical Name:N-[2-(3,4-bis-benzyloxy-phenyl)-ethyl]-succinamic-L-phenylalanyl-L-phenylalanine
CAS No.:946568-64-5
Molecular Formula:C₄₄H₄₅N₃O₇
Molecular Weight:727.857
Hs Code.:

Synonyms:N-[2-(3,4-bis-benzyloxy-phenyl)-ethyl]-succinamic-L-phenylalanyl-L-phenylalanine

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Chemical Property of N-[2-(3,4-bis-benzyloxy-phenyl)-ethyl]-succinamic-L-phenylalanyl-L-phenylalanine

Chemical Property:

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Technology Process of N-[2-(3,4-bis-benzyloxy-phenyl)-ethyl]-succinamic-L-phenylalanyl-L-phenylalanine

There total 4 articles about N-[2-(3,4-bis-benzyloxy-phenyl)-ethyl]-succinamic-L-phenylalanyl-L-phenylalanine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₉H₃₉N₃O₈

: 63-91-2,25191-15-5,658-69-5,67675-33-6
L-phenylalanine

: 946568-64-5
N-[2-(3,4-bis-benzyloxy-phenyl)-ethyl]-succinamic-L-phenylalanyl-L-phenylalanine

Guidance literature:: With sodium hydrogencarbonate; In ethanol; water; at 20 ℃; for 24h;
DOI:10.1016/j.tet.2007.02.009

Reference yield:

: 946568-63-4
N-[2-(3,4-bis-benzyloxy-phenyl)-ethyl]-succinamic-L-phenylalanine

: 946568-64-5
N-[2-(3,4-bis-benzyloxy-phenyl)-ethyl]-succinamic-L-phenylalanyl-L-phenylalanine

Guidance literature:: Multi-step reaction with 2 steps

1: DCC; DMAP / 1,2-dimethoxy-ethane / 4 h / 0 °C

2: 210 mg / NaHCO₃ / H₂O; ethanol / 24 h / 20 °C

With dmap; sodium hydrogencarbonate; dicyclohexyl-carbodiimide; In 1,2-dimethoxyethane; ethanol; water;
DOI:10.1016/j.tet.2007.02.009

Reference yield:

: 300362-70-3
3-(3,4-bis(benzyloxy)phenethylcarbamoyl) propanoic acid

: 946568-64-5
N-[2-(3,4-bis-benzyloxy-phenyl)-ethyl]-succinamic-L-phenylalanyl-L-phenylalanine

Guidance literature:: Multi-step reaction with 4 steps

1: DCC; DMAP / 1,2-dimethoxy-ethane / 24 h / 20 °C

2: 392 mg / NaHCO₃ / H₂O; ethanol / 24 h / 20 °C

3: DCC; DMAP / 1,2-dimethoxy-ethane / 4 h / 0 °C

4: 210 mg / NaHCO₃ / H₂O; ethanol / 24 h / 20 °C

With dmap; sodium hydrogencarbonate; dicyclohexyl-carbodiimide; In 1,2-dimethoxyethane; ethanol; water;
DOI:10.1016/j.tet.2007.02.009