N^2,9-bis-(p-anisyldiphenylmethyl)-O⁶-[4-(2-fluoroethoxymethyl)benzyl]guanine

Base Information

Chemical Name:N^2,9-bis-(p-anisyldiphenylmethyl)-O⁶-[4-(2-fluoroethoxymethyl)benzyl]guanine
CAS No.:868682-30-8
Molecular Formula:C₅₅H₄₈FN₅O₄
Molecular Weight:862.016
Hs Code.:

N<sup>2,9</sup>-bis-(p-anisyldiphenylmethyl)-O<sup>6</sup>-[4-(2-fluoroethoxymethyl)benzyl]guanine

Synonyms:N^2,9-bis-(p-anisyldiphenylmethyl)-O⁶-[4-(2-fluoroethoxymethyl)benzyl]guanine

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Chemical Property of N^2,9-bis-(p-anisyldiphenylmethyl)-O⁶-[4-(2-fluoroethoxymethyl)benzyl]guanine

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Technology Process of N^2,9-bis-(p-anisyldiphenylmethyl)-O⁶-[4-(2-fluoroethoxymethyl)benzyl]guanine

There total 6 articles about N^2,9-bis-(p-anisyldiphenylmethyl)-O⁶-[4-(2-fluoroethoxymethyl)benzyl]guanine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 868682-29-5
N^2,9-bis-(p-anisyldiphenylmethyl)-O⁶-[4-(hydroxymethyl)benzyl]guanine

: 762-49-2
2-fluoroethyl bromide

: 868682-30-8
N^2,9-bis-(p-anisyldiphenylmethyl)-O⁶-[4-(2-fluoroethoxymethyl)benzyl]guanine

Guidance literature:: With potassium hydroxide; In acetonitrile; at 80 ℃;
DOI:10.1016/j.bmc.2005.05.061

Reference yield:

: 868682-28-4
N^2,9-bis-(p-anisyldiphenylmethyl)-O⁶-(4-formylbenzyl)guanine

: 868682-30-8
N^2,9-bis-(p-anisyldiphenylmethyl)-O⁶-[4-(2-fluoroethoxymethyl)benzyl]guanine

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / sodium borohydride / ethanol / 3 h / 0 - 20 °C

2: 66 percent / KOH / acetonitrile / 80 °C

With potassium hydroxide; sodium tetrahydroborate; In ethanol; acetonitrile;
DOI:10.1016/j.bmc.2005.05.061

Reference yield:

: 589-29-7
p-xylylene glycol

: 868682-30-8
N^2,9-bis-(p-anisyldiphenylmethyl)-O⁶-[4-(2-fluoroethoxymethyl)benzyl]guanine

Guidance literature:: Multi-step reaction with 5 steps

1: 59 percent / sodium / 24 h / 115 °C

2: 35 percent / pyridinium chlorochromate; sodium acetate; pyridine

3: 43 percent / 4-(dimethylamino)pyridine; triethylamine / dimethylformamide / 4 h / 50 - 60 °C

4: 96 percent / sodium borohydride / ethanol / 3 h / 0 - 20 °C

5: 66 percent / KOH / acetonitrile / 80 °C

With pyridine; dmap; potassium hydroxide; sodium tetrahydroborate; sodium acetate; sodium; triethylamine; pyridinium chlorochromate; In ethanol; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.bmc.2005.05.061