1β,4α-bis(benzyloxy)-7α-hydroxy-6β-(phenylselenyl)-4aβ,8aα-decahydronaphthalene

Base Information

Chemical Name:1β,4α-bis(benzyloxy)-7α-hydroxy-6β-(phenylselenyl)-4aβ,8aα-decahydronaphthalene
CAS No.:84173-24-0
Molecular Formula:C₃₀H₃₄O₃Se
Molecular Weight:521.558
Hs Code.:

Synonyms:1β,4α-bis(benzyloxy)-7α-hydroxy-6β-(phenylselenyl)-4aβ,8aα-decahydronaphthalene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1β,4α-bis(benzyloxy)-7α-hydroxy-6β-(phenylselenyl)-4aβ,8aα-decahydronaphthalene

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Technology Process of 1β,4α-bis(benzyloxy)-7α-hydroxy-6β-(phenylselenyl)-4aβ,8aα-decahydronaphthalene

There total 11 articles about 1β,4α-bis(benzyloxy)-7α-hydroxy-6β-(phenylselenyl)-4aβ,8aα-decahydronaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 79782-37-9,84173-23-9
Acetic acid (2S,4aS,5R,8R,8aS)-5,8-bis-benzyloxy-3-phenylselanyl-decahydro-naphthalen-2-yl ester

: 79782-38-0,84173-24-0
(2S,4aS,5R,8R,8aS)-5,8-Bis-benzyloxy-3-phenylselanyl-decahydro-naphthalen-2-ol

Guidance literature:: With potassium hydroxide; In methanol; diethyl ether; at 25 ℃; for 2h;
DOI:10.1021/ja00411a063

Reference yield: 88.0%

: 79782-37-9,84173-23-9
7α-acetoxy-1β,4α-bis(benzyloxy)-6β-(phenylselenyl)-4aβ,8aα-decahydronaphthalene

: 84173-24-0
1β,4α-bis(benzyloxy)-7α-hydroxy-6β-(phenylselenyl)-4aβ,8aα-decahydronaphthalene

Guidance literature:: With potassium hydroxide; In methanol; diethyl ether; at 25 ℃; for 2h;
DOI:10.1021/ja00341a046

Reference yield:

: 34837-55-3
Phenylselenyl bromide

: 79782-38-0,84173-24-0
(2S,4aS,5R,8R,8aS)-5,8-Bis-benzyloxy-3-phenylselanyl-decahydro-naphthalen-2-ol

Guidance literature:: Multi-step reaction with 2 steps

1: KOAc / 1 h / 25 °C

2: 89 percent / KOH / methanol; diethyl ether / 2 h / 25 °C

With potassium hydroxide; potassium acetate; In methanol; diethyl ether;
DOI:10.1021/ja00411a063