7α-acetoxy-1β,4α-bis(benzyloxy)-6β-(phenylselenyl)-4aβ,8aα-decahydronaphthalene

Base Information

Chemical Name:7α-acetoxy-1β,4α-bis(benzyloxy)-6β-(phenylselenyl)-4aβ,8aα-decahydronaphthalene
CAS No.:79782-37-9
Molecular Formula:C₃₂H₃₆O₄Se
Molecular Weight:563.595
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 7α-acetoxy-1β,4α-bis(benzyloxy)-6β-(phenylselenyl)-4aβ,8aα-decahydronaphthalene

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Technology Process of 7α-acetoxy-1β,4α-bis(benzyloxy)-6β-(phenylselenyl)-4aβ,8aα-decahydronaphthalene

There total 7 articles about 7α-acetoxy-1β,4α-bis(benzyloxy)-6β-(phenylselenyl)-4aβ,8aα-decahydronaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1666-13-3
diphenyl diselenide

: 79782-37-9,84173-23-9
7α-acetoxy-1β,4α-bis(benzyloxy)-6β-(phenylselenyl)-4aβ,8aα-decahydronaphthalene

Guidance literature:: Multi-step reaction with 2 steps

1: Br₂ / acetic acid / 0.17 h / Ambient temperature

2: 32 g / acetic acid / 1 h / 25 °C

With bromine; In acetic acid;
DOI:10.1021/ja00341a046

Reference yield:

: 2906-93-6,3198-51-4,6102-42-7,36159-09-8,54963-84-7,84275-37-6
(+/-)-1,4,5,8,9,10-trans-hexahydronaphthalene-1,4-dione

: 79782-37-9,84173-23-9
7α-acetoxy-1β,4α-bis(benzyloxy)-6β-(phenylselenyl)-4aβ,8aα-decahydronaphthalene

Guidance literature:: Multi-step reaction with 3 steps

1: 18.67 g / Aureobasidium pullulans NRRL Y-12610 / H₂O / 72 °C

2: 99 percent / 1.) NaH / dimethylsulfoxide / 1.) RT, 30 min, 2.) RT, 3 h

3: 32 g / acetic acid / 1 h / 25 °C

With Aureobasidium pullulans NRRL Y-12610; sodium hydride; In water; acetic acid; dimethyl sulfoxide;
DOI:10.1021/ja00341a046

Reference yield:

: 2906-93-6,3198-51-4,6102-42-7,36159-09-8,54963-84-7,84275-37-6
(+/-)-1,4,5,8,9,10-trans-hexahydronaphthalene-1,4-dione

: 79782-37-9,84173-23-9
Acetic acid (2S,4aS,5R,8R,8aS)-5,8-bis-benzyloxy-3-phenylselanyl-decahydro-naphthalen-2-yl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 33 percent / Aureobasidium pullulans NRRL Y-12610

2: 99 percent / NaH / dimethylsulfoxide / 25 °C

3: KOAc / 1 h / 25 °C

With Aureobasidium pullulans NRRL Y-12610; potassium acetate; sodium hydride; In dimethyl sulfoxide;
DOI:10.1021/ja00411a063