(S)-N-glycidyl-N-(2-methylene-5-(2-nitrobenzenesulfonamido)pentyl)-2-nitrobenzenesulfonamide

Base Information

Chemical Name:(S)-N-glycidyl-N-(2-methylene-5-(2-nitrobenzenesulfonamido)pentyl)-2-nitrobenzenesulfonamide
CAS No.:1609184-07-7
Molecular Formula:C₂₁H₂₄N₄O₉S₂
Molecular Weight:540.575
Hs Code.:

Synonyms:(S)-N-glycidyl-N-(2-methylene-5-(2-nitrobenzenesulfonamido)pentyl)-2-nitrobenzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-N-glycidyl-N-(2-methylene-5-(2-nitrobenzenesulfonamido)pentyl)-2-nitrobenzenesulfonamide

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Technology Process of (S)-N-glycidyl-N-(2-methylene-5-(2-nitrobenzenesulfonamido)pentyl)-2-nitrobenzenesulfonamide

There total 7 articles about (S)-N-glycidyl-N-(2-methylene-5-(2-nitrobenzenesulfonamido)pentyl)-2-nitrobenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1609184-06-6
(S)-N-(5-(N-allyloxycarbonyl-2-nitrobenzenesulfonamido)-2-methylenepentyl)-N-glycidyl-2-nitrobenzenesulfonamide

: 1609184-07-7
(S)-N-glycidyl-N-(2-methylene-5-(2-nitrobenzenesulfonamido)pentyl)-2-nitrobenzenesulfonamide

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; acetic acid; HSiPh₃; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ol5010033

Reference yield:

: 1609184-04-4
(S)-N-(5-((tert-butyldimethylsilyl)oxy)-2-methylenepentyl)-N-glycidyl-2-nitrobenzenesulfonamide

: 1609184-07-7
(S)-N-glycidyl-N-(2-methylene-5-(2-nitrobenzenesulfonamido)pentyl)-2-nitrobenzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 9 h / 20 °C / Inert atmosphere

2: triphenylphosphine; azodicarboxylic acid bis(2-methoxyethyl) ester / tetrahydrofuran / 0.17 h / 20 °C / Inert atmosphere

3: HSiPh₃; tetrakis(triphenylphosphine) palladium⁽⁰⁾; acetic acid / 2 h / 20 °C / Inert atmosphere

With azodicarboxylic acid bis(2-methoxyethyl) ester; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrabutyl ammonium fluoride; acetic acid; triphenylphosphine; HSiPh₃; In tetrahydrofuran;
DOI:10.1021/ol5010033

Reference yield:

: 1609184-05-5
(S)-N-glycidyl-N-(5-hydroxy-2-methylenepentyl)-2-nitrobenzenesulfonamide

: 1609184-07-7
(S)-N-glycidyl-N-(2-methylene-5-(2-nitrobenzenesulfonamido)pentyl)-2-nitrobenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: triphenylphosphine; azodicarboxylic acid bis(2-methoxyethyl) ester / tetrahydrofuran / 0.17 h / 20 °C / Inert atmosphere

2: HSiPh₃; tetrakis(triphenylphosphine) palladium⁽⁰⁾; acetic acid / 2 h / 20 °C / Inert atmosphere

With azodicarboxylic acid bis(2-methoxyethyl) ester; tetrakis(triphenylphosphine) palladium⁽⁰⁾; acetic acid; triphenylphosphine; HSiPh₃; In tetrahydrofuran;
DOI:10.1021/ol5010033