(1'R,2'R,2S,4S,5R)-N-ethoxycarbonyl-2-(1'-ethoxycarbonyl-2'-furyl-2'-hydroxyethyl)-4-methyl-5-phenyl-1,3-oxazolidine

Base Information

Chemical Name:(1'R,2'R,2S,4S,5R)-N-ethoxycarbonyl-2-(1'-ethoxycarbonyl-2'-furyl-2'-hydroxyethyl)-4-methyl-5-phenyl-1,3-oxazolidine
CAS No.:223394-29-4
Molecular Formula:C₂₂H₂₇NO₇
Molecular Weight:417.459
Hs Code.:

Synonyms:(1'R,2'R,2S,4S,5R)-N-ethoxycarbonyl-2-(1'-ethoxycarbonyl-2'-furyl-2'-hydroxyethyl)-4-methyl-5-phenyl-1,3-oxazolidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1'R,2'R,2S,4S,5R)-N-ethoxycarbonyl-2-(1'-ethoxycarbonyl-2'-furyl-2'-hydroxyethyl)-4-methyl-5-phenyl-1,3-oxazolidine

Chemical Property:

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Technology Process of (1'R,2'R,2S,4S,5R)-N-ethoxycarbonyl-2-(1'-ethoxycarbonyl-2'-furyl-2'-hydroxyethyl)-4-methyl-5-phenyl-1,3-oxazolidine

There total 1 articles about (1'R,2'R,2S,4S,5R)-N-ethoxycarbonyl-2-(1'-ethoxycarbonyl-2'-furyl-2'-hydroxyethyl)-4-methyl-5-phenyl-1,3-oxazolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98-01-1
furfural

: 223394-25-0
(2S,4S,5R)-N-ethoxycarbonyl-2-(1'-ethoxycarbonylmethylen)-5-phenyl-4-methyl-1,3-oxazolidine

: (4S,5R)-N-(2'-ethoxycarbonylethenyl)-5-phenyl-4-methyl-oxazolidinone

: 223394-29-4
(1'R,2'R,2S,4S,5R)-N-ethoxycarbonyl-2-(1'-ethoxycarbonyl-2'-furyl-2'-hydroxyethyl)-4-methyl-5-phenyl-1,3-oxazolidine

Guidance literature:: With tert-butyl formate; tert.-butyl lithium; Yield given; Multistep reaction. Yields of byproduct given; 1.) THF, -78 deg C, 15 min, 2.) THF, 20 deg C, 25 min;
DOI:10.1016/S0040-4020(99)00046-0

Reference yield: 80.0%

: 223394-29-4
(1'R,2'R,2S,4S,5R)-N-ethoxycarbonyl-2-(1'-ethoxycarbonyl-2'-furyl-2'-hydroxyethyl)-4-methyl-5-phenyl-1,3-oxazolidine

: 223394-32-9
(1R,2S,5R,6R)-3-aza-1-phenyl-6-furyl-5-hydroxymethyl-2,3-dimethyl-1,6-hexanediol

Guidance literature:: With lithium aluminium tetrahydride; aluminium trichloride; In tetrahydrofuran; at 0 ℃; for 0.25h;
DOI:10.1016/S0040-4020(99)00046-0

Reference yield:

: 223394-29-4
(1'R,2'R,2S,4S,5R)-N-ethoxycarbonyl-2-(1'-ethoxycarbonyl-2'-furyl-2'-hydroxyethyl)-4-methyl-5-phenyl-1,3-oxazolidine

: 223394-34-1
(4R,5R,3'S,4'R)-5-(2'-aza-2',3'-dimethyl-4'-hydroxy-4'-phenyl-butyl)-2,2-dimethyl-4-furyl-1,3-dioxane

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / LiAlH₄, AlCl₃ / tetrahydrofuran / 0.25 h / 0 °C

2: pTsOH / acetone / 12 h / Heating

With lithium aluminium tetrahydride; aluminium trichloride; toluene-4-sulfonic acid; In tetrahydrofuran; acetone;
DOI:10.1016/S0040-4020(99)00046-0