(±)-2-((1-(tert-butoxycarbonylamino)-4-methylpent-2-yl)oxy)benzaldehyde

Base Information

Chemical Name:(±)-2-((1-(tert-butoxycarbonylamino)-4-methylpent-2-yl)oxy)benzaldehyde
CAS No.:1318907-38-8
Molecular Formula:C₁₈H₂₇NO₄
Molecular Weight:321.417
Hs Code.:

Synonyms:(±)-2-((1-(tert-butoxycarbonylamino)-4-methylpent-2-yl)oxy)benzaldehyde

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Chemical Property of (±)-2-((1-(tert-butoxycarbonylamino)-4-methylpent-2-yl)oxy)benzaldehyde

Chemical Property:

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Technology Process of (±)-2-((1-(tert-butoxycarbonylamino)-4-methylpent-2-yl)oxy)benzaldehyde

There total 3 articles about (±)-2-((1-(tert-butoxycarbonylamino)-4-methylpent-2-yl)oxy)benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1318907-33-3
(±)-N-methyl-N-methoxy-2-{[1-(tert-butoxycarbonylamino)-4-methylpent-2-yl]oxy}benzamide

: 1318907-38-8
(±)-2-((1-(tert-butoxycarbonylamino)-4-methylpent-2-yl)oxy)benzaldehyde

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether; at 0 ℃; for 2h; Inert atmosphere;
DOI:10.3762/bjoc.7.109

Reference yield:

: 2-hydroxy-N-methoxy-N-methylbenzamide

: 1318907-38-8
(±)-2-((1-(tert-butoxycarbonylamino)-4-methylpent-2-yl)oxy)benzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: di-tert-butyl-diazodicarboxylate; triphenylphosphine / tetrahydrofuran / 6.83 h / 0 °C / Inert atmosphere

2: lithium aluminium tetrahydride / tetrahydrofuran; diethyl ether / 2 h / 0 °C / Inert atmosphere

With lithium aluminium tetrahydride; di-tert-butyl-diazodicarboxylate; triphenylphosphine; In tetrahydrofuran; diethyl ether; 1: Mitsunobu reaction;
DOI:10.3762/bjoc.7.109

Reference yield:

: 69-72-7,25496-36-0,8052-31-1
salicylic acid

: 1318907-38-8
(±)-2-((1-(tert-butoxycarbonylamino)-4-methylpent-2-yl)oxy)benzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1,1'-carbonyldiimidazole / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

1.2: 6 h / 20 °C / Inert atmosphere

2.1: di-tert-butyl-diazodicarboxylate; triphenylphosphine / tetrahydrofuran / 6.83 h / 0 °C / Inert atmosphere

3.1: lithium aluminium tetrahydride / tetrahydrofuran; diethyl ether / 2 h / 0 °C / Inert atmosphere

With lithium aluminium tetrahydride; di-tert-butyl-diazodicarboxylate; triphenylphosphine; 1,1'-carbonyldiimidazole; In tetrahydrofuran; diethyl ether; 2.1: Mitsunobu reaction;
DOI:10.3762/bjoc.7.109