(E)-(2-(1,2-bis(4-chlorophenyl)vinyl)phenyl)phosphonic acid bis(diethylamide)

Base Information

Chemical Name:(E)-(2-(1,2-bis(4-chlorophenyl)vinyl)phenyl)phosphonic acid bis(diethylamide)
CAS No.:1451210-98-2
Molecular Formula:C₂₈H₃₃Cl₂N₂OP
Molecular Weight:515.463
Hs Code.:

Synonyms:(E)-(2-(1,2-bis(4-chlorophenyl)vinyl)phenyl)phosphonic acid bis(diethylamide)

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Chemical Property of (E)-(2-(1,2-bis(4-chlorophenyl)vinyl)phenyl)phosphonic acid bis(diethylamide)

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Technology Process of (E)-(2-(1,2-bis(4-chlorophenyl)vinyl)phenyl)phosphonic acid bis(diethylamide)

There total 2 articles about (E)-(2-(1,2-bis(4-chlorophenyl)vinyl)phenyl)phosphonic acid bis(diethylamide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1820-42-4
bis(4-chlorophenyl)acetylene

: 4519-35-1
N,N,N’,N’-tetraethyl-P-phenyl-phosphonic diamide

: 1451210-98-2
(E)-(2-(1,2-bis(4-chlorophenyl)vinyl)phenyl)phosphonic acid bis(diethylamide)

Guidance literature:: With silver hexafluoroantimonate; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; copper diacetate; Trimethylacetic acid; In 1,2-dichloro-ethane; at 110 ℃; for 24h; stereoselective reaction; Inert atmosphere;
DOI:10.1021/ol402053n

Reference yield:

: 824-72-6
P,P-dichlorophenylphosphine oxide

: 1451210-98-2
(E)-(2-(1,2-bis(4-chlorophenyl)vinyl)phenyl)phosphonic acid bis(diethylamide)

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; dmap / dichloromethane / 0 - 20 °C

2: copper diacetate; silver hexafluoroantimonate; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; Trimethylacetic acid / 1,2-dichloro-ethane / 24 h / 110 °C / Inert atmosphere

With dmap; silver hexafluoroantimonate; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; copper diacetate; triethylamine; Trimethylacetic acid; In dichloromethane; 1,2-dichloro-ethane;
DOI:10.1021/ol402053n