4-([2,2'-bithiophen]-5-yl)-N,N-bis[4-(3,6-di-tert-butylcarbazol-9-yl)phenyl]aniline

Base Information

• Chemical Name: 4-([2,2'-bithiophen]-5-yl)-N,N-bis[4-(3,6-di-tert-butylcarbazol-9-yl)phenyl]aniline
• CAS No.: 1439565-81-7
• Molecular Formula: C₆₆H₆₅N₃S₂
• Molecular Weight: 964.394

Synonyms:4-([2,2'-bithiophen]-5-yl)-N,N-bis[4-(3,6-di-tert-butylcarbazol-9-yl)phenyl]aniline

Chemical Property of 4-([2,2'-bithiophen]-5-yl)-N,N-bis[4-(3,6-di-tert-butylcarbazol-9-yl)phenyl]aniline

Chemical Property:

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Technology Process of 4-([2,2'-bithiophen]-5-yl)-N,N-bis[4-(3,6-di-tert-butylcarbazol-9-yl)phenyl]aniline

There total 2 articles about 4-([2,2'-bithiophen]-5-yl)-N,N-bis[4-(3,6-di-tert-butylcarbazol-9-yl)phenyl]aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

thiophene boronic acid (6165-68-0) + 4,7-bis{5-(N,N-bis[4-(3,6-di-tert-butylcarbazol-N-yl)phenyl]aminophenyl)-thien-2-yl}-2,1,3-benzothiadiazole (1429922-07-5) → 4-([2,2'-bithiophen]-5-yl)-N,N-bis[4-(3,6-di-tert-butylcarbazol-9-yl)phenyl]aniline (1439565-81-7)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In tetrahydrofuran; water; for 24h; Inert atmosphere; Reflux;

DOI:10.1002/ejoc.201201479

Reference yield: 63.0%

thiophene boronic acid (6165-68-0) + N,N-bis(4-(3,6-di-tert-butylcarbazol-9-yl)phenyl)-4-(thiophen-2-yl)aniline (1429922-06-4) → 4-([2,2'-bithiophen]-5-yl)-N,N-bis[4-(3,6-di-tert-butylcarbazol-9-yl)phenyl]aniline (1439565-81-7)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In tetrahydrofuran; for 24h; Reflux; Inert atmosphere;

DOI:10.1021/jo4008332

Reference yield: 87.0%

4-([2,2'-bithiophen]-5-yl)-N,N-bis[4-(3,6-di-tert-butylcarbazol-9-yl)phenyl]aniline (1439565-81-7) → 4-(5'-bromo-2,2’-bithiophen-5-yl)-N,N-bis(4-(3,6-di-tert-butylcarbazol-9-yl)phenyl)aniline (1439565-89-5)

Guidance literature:

With N-Bromosuccinimide; In tetrahydrofuran; at 20 ℃; for 1h; Inert atmosphere;

DOI:10.1002/ejoc.201201479

upstream raw materials:

thiophene boronic acid

4,7-bis{5-(N,N-bis[4-(3,6-di-tert-butylcarbazol-N-yl)phenyl]aminophenyl)-thien-2-yl}-2,1,3-benzothiadiazole

N,N-bis(4-(3,6-di-tert-butylcarbazol-9-yl)phenyl)-4-(thiophen-2-yl)aniline

Downstream raw materials:

4-(5'-bromo-2,2’-bithiophen-5-yl)-N,N-bis(4-(3,6-di-tert-butylcarbazol-9-yl)phenyl)aniline

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