4,7-bis{5-(N,N-bis[4-(3,6-di-tert-butylcarbazol-N-yl)phenyl]aminophenyl)-thien-2-yl}-2,1,3-benzothiadiazole

Base Information

Chemical Name:4,7-bis{5-(N,N-bis[4-(3,6-di-tert-butylcarbazol-N-yl)phenyl]aminophenyl)-thien-2-yl}-2,1,3-benzothiadiazole
CAS No.:1429922-07-5
Molecular Formula:C₆₂H₆₂BrN₃S
Molecular Weight:961.164
Hs Code.:

Synonyms:4,7-bis{5-(N,N-bis[4-(3,6-di-tert-butylcarbazol-N-yl)phenyl]aminophenyl)-thien-2-yl}-2,1,3-benzothiadiazole

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Chemical Property of 4,7-bis{5-(N,N-bis[4-(3,6-di-tert-butylcarbazol-N-yl)phenyl]aminophenyl)-thien-2-yl}-2,1,3-benzothiadiazole

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Technology Process of 4,7-bis{5-(N,N-bis[4-(3,6-di-tert-butylcarbazol-N-yl)phenyl]aminophenyl)-thien-2-yl}-2,1,3-benzothiadiazole

There total 2 articles about 4,7-bis{5-(N,N-bis[4-(3,6-di-tert-butylcarbazol-N-yl)phenyl]aminophenyl)-thien-2-yl}-2,1,3-benzothiadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1429922-06-4
N,N-bis(4-(3,6-di-tert-butylcarbazol-9-yl)phenyl)-4-(thiophen-2-yl)aniline

: 1429922-07-5
4,7-bis{5-(N,N-bis[4-(3,6-di-tert-butylcarbazol-N-yl)phenyl]aminophenyl)-thien-2-yl}-2,1,3-benzothiadiazole

Guidance literature:: With N-Bromosuccinimide; In tetrahydrofuran; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1039/c3cc41154k

Reference yield: 91.0%

: 128-08-5
N-Bromosuccinimide

: 1429922-06-4
N,N-bis(4-(3,6-di-tert-butylcarbazol-9-yl)phenyl)-4-(thiophen-2-yl)aniline

: 1429922-07-5
4,7-bis{5-(N,N-bis[4-(3,6-di-tert-butylcarbazol-N-yl)phenyl]aminophenyl)-thien-2-yl}-2,1,3-benzothiadiazole

Guidance literature:: In tetrahydrofuran; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/jo4008332

Reference yield: 63.0%

: 6165-68-0
thiophene boronic acid

: 1429922-07-5
4,7-bis{5-(N,N-bis[4-(3,6-di-tert-butylcarbazol-N-yl)phenyl]aminophenyl)-thien-2-yl}-2,1,3-benzothiadiazole

: 1439565-81-7
4-([2,2'-bithiophen]-5-yl)-N,N-bis[4-(3,6-di-tert-butylcarbazol-9-yl)phenyl]aniline

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In tetrahydrofuran; water; for 24h; Inert atmosphere; Reflux;
DOI:10.1002/ejoc.201201479