C₂₂H₃₄OSi

Base Information

• Chemical Name: C₂₂H₃₄OSi
• CAS No.: 1008533-99-0
• Molecular Formula: C₂₂H₃₄OSi
• Molecular Weight: 342.597
• Mol file: 1008533-99-0.mol

Synonyms:C₂₂H₃₄OSi

Chemical Property of C₂₂H₃₄OSi

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₂₂H₃₄OSi

There total 2 articles about C₂₂H₃₄OSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

C13H28OSi2 (1174908-09-8) + 1-phenylpent-2-en-1-one (61752-65-6,61752-66-7,19738-86-4) → C22H34OSi (1008533-99-0)

Guidance literature:

With [Rh(OH)(R)-binap]2; In 1,4-dioxane; water; at 60 ℃; for 12h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;

DOI:10.1021/ol901119d

Reference yield:

tris-iso-propylsilyl acetylene (89343-06-6) + (E)-1-phenyl-2-penten-1-one (61752-66-7) → C22H34OSi + C22H34OSi (1008533-99-0)

Guidance literature:

(R)-((4,4’-bi-1,3-benzodioxole)-5,5’-diyl)bis(bis(3,5-di-t-butyl-4-methoxyphenyl))phosphine; In 1,4-dioxane; at 80 ℃; for 24h; Title compound not separated from byproducts.;

DOI:10.1021/ja710540s

upstream raw materials:

tris-iso-propylsilyl acetylene

(E)-1-phenyl-2-penten-1-one

C₁₃H₂₈OSi₂

1-phenylpent-2-en-1-one