1-(2,3,4-trimethoxyphenyl)-2-{[5-(3,4,5-trimethoxyphenyl)-1,3,4-thiazdiazol-2-yl]thio}ethanone

Base Information

Chemical Name:1-(2,3,4-trimethoxyphenyl)-2-{[5-(3,4,5-trimethoxyphenyl)-1,3,4-thiazdiazol-2-yl]thio}ethanone
CAS No.:892440-74-3
Molecular Formula:C₂₂H₂₄N₂O₇S₂
Molecular Weight:492.574
Hs Code.:

Synonyms:1-(2,3,4-trimethoxyphenyl)-2-{[5-(3,4,5-trimethoxyphenyl)-1,3,4-thiazdiazol-2-yl]thio}ethanone

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Chemical Property of 1-(2,3,4-trimethoxyphenyl)-2-{[5-(3,4,5-trimethoxyphenyl)-1,3,4-thiazdiazol-2-yl]thio}ethanone

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Technology Process of 1-(2,3,4-trimethoxyphenyl)-2-{[5-(3,4,5-trimethoxyphenyl)-1,3,4-thiazdiazol-2-yl]thio}ethanone

There total 4 articles about 1-(2,3,4-trimethoxyphenyl)-2-{[5-(3,4,5-trimethoxyphenyl)-1,3,4-thiazdiazol-2-yl]thio}ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.7%

: 299465-16-0
5-(3,4,5-trimethoxyphenyl)-1,3,4-thiadiazole-2-thiol

: 54109-14-7
α-bromo-2',3',4'-trimethoxyacetophenone

: 892440-74-3
1-(2,3,4-trimethoxyphenyl)-2-{[5-(3,4,5-trimethoxyphenyl)-1,3,4-thiazdiazol-2-yl]thio}ethanone

Guidance literature:: 5-(3,4,5-trimethoxyphenyl)-1,3,4-thiadiazole-2-thiol; With sodium hydroxide; at 20 ℃; for 0.166667h;

α-bromo-2',3',4'-trimethoxyacetophenone; With indium; at 20 ℃; for 3h;
DOI:10.1002/jhet.5570430409

Reference yield:

: 1916-07-0
3,4,5-trimethoxybenzoic acid methyl ester

: 892440-74-3
1-(2,3,4-trimethoxyphenyl)-2-{[5-(3,4,5-trimethoxyphenyl)-1,3,4-thiazdiazol-2-yl]thio}ethanone

Guidance literature:: Multi-step reaction with 4 steps

1.1: 89 percent / NH₂NH₂*H₂O / methanol / 5 h / Heating

2.1: 66.5 percent / potassium hydroxide / methanol / 2 h / Heating

3.1: 43.8 percent / sulfuric acid / 1.5 h / -5 - 0 °C

4.1: aq. NaOH / 0.17 h / 20 °C

4.2: 83.7 percent / indium / 3 h / 20 °C

With potassium hydroxide; sodium hydroxide; sulfuric acid; hydrazine hydrate; In methanol;
DOI:10.1002/jhet.5570430409

Reference yield:

: 3291-03-0
3,4,5-trimethoxybenzohydrazide

: 892440-74-3
1-(2,3,4-trimethoxyphenyl)-2-{[5-(3,4,5-trimethoxyphenyl)-1,3,4-thiazdiazol-2-yl]thio}ethanone

Guidance literature:: Multi-step reaction with 3 steps

1.1: 66.5 percent / potassium hydroxide / methanol / 2 h / Heating

2.1: 43.8 percent / sulfuric acid / 1.5 h / -5 - 0 °C

3.1: aq. NaOH / 0.17 h / 20 °C

3.2: 83.7 percent / indium / 3 h / 20 °C

With potassium hydroxide; sodium hydroxide; sulfuric acid; In methanol;
DOI:10.1002/jhet.5570430409