Technology Process of C56H36
There total 5 articles about C56H36 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
Aliquat 336; calcium carbonate;
tetrakis(triphenylphosphine) palladium(0);
In
water; toluene;
at 120 ℃;
for 6h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium carbonate / trans-bis(triphenylphosphine)palladium dichloride / toluene; water / 3 h / 120 °C
2.1: n-butyllithium / hexane; tetrahydrofuran / 1 h / -78 °C / Inert atmosphere
2.2: 25 °C
3.1: Aliquat 336; calcium carbonate / tetrakis(triphenylphosphine) palladium(0) / toluene; water / 6 h / 120 °C
With
n-butyllithium; Aliquat 336; sodium carbonate; calcium carbonate;
tetrakis(triphenylphosphine) palladium(0); trans-bis(triphenylphosphine)palladium dichloride;
In
tetrahydrofuran; hexane; water; toluene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium carbonate / trans-bis(triphenylphosphine)palladium dichloride / toluene; water / 3 h / 120 °C
2.1: n-butyllithium / hexane; tetrahydrofuran / 1 h / -78 °C / Inert atmosphere
2.2: 25 °C
3.1: Aliquat 336; calcium carbonate / tetrakis(triphenylphosphine) palladium(0) / toluene; water / 6 h / 120 °C
With
n-butyllithium; Aliquat 336; sodium carbonate; calcium carbonate;
tetrakis(triphenylphosphine) palladium(0); trans-bis(triphenylphosphine)palladium dichloride;
In
tetrahydrofuran; hexane; water; toluene;