Technology Process of C34H35BrO7
There total 6 articles about C34H35BrO7 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine;
In
1,2-dichloro-ethane;
DOI:10.1021/ol015733i
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: pyridine
2.1: m-CPBA / pyridine
3.1: BF3*OEt2 / toluene
3.2: 76 percent / p-TsOH / CH2Cl2 / 72 h / 20 °C
4.1: 89 percent / Huenig base; TBAI / 1,2-dichloro-ethane
With
boron trifluoride diethyl etherate; tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid;
In
pyridine; 1,2-dichloro-ethane; toluene;
DOI:10.1021/ol015733i
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: HCl / methanol; tetrahydrofuran
2.1: pyridine
3.1: m-CPBA / pyridine
4.1: BF3*OEt2 / toluene
4.2: 76 percent / p-TsOH / CH2Cl2 / 72 h / 20 °C
5.1: 89 percent / Huenig base; TBAI / 1,2-dichloro-ethane
With
hydrogenchloride; boron trifluoride diethyl etherate; tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; pyridine; methanol; 1,2-dichloro-ethane; toluene;
DOI:10.1021/ol015733i