C₃₁H₃₀O₄S

Base Information

Chemical Name:C₃₁H₃₀O₄S
CAS No.:1602921-35-6
Molecular Formula:C₃₁H₃₀O₄S
Molecular Weight:498.643
Hs Code.:

C<sub>31</sub>H<sub>30</sub>O<sub>4</sub>S

Synonyms:C₃₁H₃₀O₄S

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Chemical Property of C₃₁H₃₀O₄S

Chemical Property:

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Technology Process of C₃₁H₃₀O₄S

There total 7 articles about C₃₁H₃₀O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1602921-28-7
p-tolyl 4,6-O-benzylidene-2-deoxy-1-thio-β-D-galactopyranoside

: 939-26-4
2-bromomethylnaphthyl bromide

: 1602921-35-6
C₃₁H₃₀O₄S

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 1.5h; Inert atmosphere;
DOI:10.1002/ejoc.201400006

Reference yield:

: 10257-28-0
D-Galactose

: 1602921-35-6
C₃₁H₃₀O₄S

Guidance literature:: Multi-step reaction with 7 steps

1: sulfuric acid / 42 h / -20 - 0 °C

2: hydrogen bromide; acetic acid / 3 h / 20 °C

3: zinc; sodium dihydrogenphosphate / acetone / 6 h / 20 °C

4: hydrogenchloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 12 h / 20 °C

5: methanol; sodium / 3.5 h / 20 °C

6: toluene-4-sulfonic acid / acetonitrile / 1 h / 20 °C

7: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1.5 h / 0 - 20 °C / Inert atmosphere

With hydrogenchloride; methanol; sodium dihydrogenphosphate; sulfuric acid; hydrogen bromide; sodium; sodium hydride; toluene-4-sulfonic acid; acetic acid; N-ethyl-N,N-diisopropylamine; zinc; In dichloromethane; N,N-dimethyl-formamide; acetone; acetonitrile; mineral oil;
DOI:10.1002/ejoc.201400006

Reference yield:

: 25878-60-8
D-galactose pentaacetate

: 1602921-35-6
C₃₁H₃₀O₄S

Guidance literature:: Multi-step reaction with 6 steps

1: hydrogen bromide; acetic acid / 3 h / 20 °C

2: zinc; sodium dihydrogenphosphate / acetone / 6 h / 20 °C

3: hydrogenchloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 12 h / 20 °C

4: methanol; sodium / 3.5 h / 20 °C

5: toluene-4-sulfonic acid / acetonitrile / 1 h / 20 °C

6: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1.5 h / 0 - 20 °C / Inert atmosphere

With hydrogenchloride; methanol; sodium dihydrogenphosphate; hydrogen bromide; sodium; sodium hydride; toluene-4-sulfonic acid; acetic acid; N-ethyl-N,N-diisopropylamine; zinc; In dichloromethane; N,N-dimethyl-formamide; acetone; acetonitrile; mineral oil;
DOI:10.1002/ejoc.201400006