2,3-dibromo-3-phenylpropan-1-ol

Base Information

• Chemical Name: 2,3-dibromo-3-phenylpropan-1-ol
• CAS No.: 36808-12-5
• Molecular Formula: C₉H₁₀Br₂O
• Molecular Weight: 293.986
• Mol file: 36808-12-5.mol

Synonyms:2,3-dibromo-3-phenylpropan-1-ol

Chemical Property of 2,3-dibromo-3-phenylpropan-1-ol

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

2,3-Dibromo-3-phenyl-1-propanol 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,3-dibromo-3-phenylpropan-1-ol

There total 18 articles about 2,3-dibromo-3-phenylpropan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

(2E)-3-phenyl-2-propen-1-ol (4407-36-7) → rac-(2R,3S)-2,3-dibromo-3-phenylpropan-1-ol (36808-12-5,83263-29-0,142052-64-0)

Guidance literature:

With 4-dimethylaminopyridine tribromide; In acetic acid; for 0.25h; Ambient temperature;

Reference yield: 98.0%

3-Phenylpropenol (104-54-1) → 2,3-dibromo-3-phenylpropan-1-ol (36808-12-5)

Guidance literature:

With sodium periodate; acetic acid; lithium bromide; at 25 ℃;

DOI:10.1021/ol0358206

Reference yield: 93.0%

(2E)-3-phenyl-2-propen-1-ol (4407-36-7) → (E)-3-phenylpropenal (14371-10-9) + 2,3-dibromo-3-phenylpropan-1-ol (36808-12-5)

Guidance literature:

With 1-[4-(diacetoxyiodo)benzyl]-3-methylimidazolium BF₄; 1-ethyl-3-methylimidazolium tetrafluoroborate; sodium bromide; at 30 ℃; for 4h;

DOI:10.1002/anie.200461889

upstream raw materials:

3-Phenylpropenol

(2E)-3-phenyl-2-propen-1-ol

(E)-3-phenylpropenal

methyl cinnamate

Downstream raw materials:

1-phenyl-propane-1,2,3-triol

(1,2,3-tribromo-propyl)-benzene

acetic acid-((2RS,3SR)-2,3-dibromo-3-phenyl-propyl ester)

benzoic acid-((2RS,3SR)-2,3-dibromo-3-phenyl-propyl ester)