Technology Process of (3,4-dihydronaphthalen-1-yl)(phenyl)methanone
There total 7 articles about (3,4-dihydronaphthalen-1-yl)(phenyl)methanone which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
(Z)-((2-(2,3-dihydro-1H-inden-1-yl)-1-phenylvinyl)oxy)trimethylsilane;
With
trimethylsilyl trifluoromethanesulfonate; [bis(acetoxy)iodo]benzene;
In
dichloromethane;
at -78 ℃;
for 0.5h;
Inert atmosphere;
Schlenk technique;
With
triethylamine;
In
dichloromethane;
at -78 - 20 ℃;
for 1.08333h;
stereoselective reaction;
Inert atmosphere;
Schlenk technique;
DOI:10.1021/acs.orglett.1c00251
- Guidance literature:
-
With
2-mesityl-6,7-dihydro-5H-pyrrolo[2,1-c][1,2,4]triazol-2-ium tetrafluoroborate; tris(2,2-bipyridine)ruthenium(II) hexafluorophosphate; sodium p-chlorobenzenesulphinate; caesium carbonate; 1-methyl-2,3,4,6,7,8-hexahydro-1H-pyrimido[1,2-a]pyrimidine;
In
acetonitrile;
at 20 ℃;
for 24h;
Time;
regioselective reaction;
Irradiation;
Inert atmosphere;
Schlenk technique;
DOI:10.1021/jacs.1c01022
- Guidance literature:
-
benzoyl chloride;
With
indium; chloro-trimethyl-silane; ethylene dibromide; lithium chloride;
In
1-methyl-pyrrolidin-2-one;
at 40 ℃;
for 3h;
Inert atmosphere;
3,4-dihydro-1-naphthyl triflate;
With
tris-(dibenzylideneacetone)dipalladium(0);
In
1-methyl-pyrrolidin-2-one;
at 25 ℃;
for 6h;
Inert atmosphere;
DOI:10.1021/ol500003g
