Diethyl-α-trichloromethylbenzyl Phosphate

Base Information

• Chemical Name: Diethyl-α-trichloromethylbenzyl Phosphate
• CAS No.: 72945-89-2
• Molecular Formula: C₁₂H₁₆Cl₃O₄P
• Molecular Weight: 361.589
• Mol file: 72945-89-2.mol

Synonyms:Diethyl-α-trichloromethylbenzyl Phosphate

Chemical Property of Diethyl-α-trichloromethylbenzyl Phosphate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Diethyl-α-trichloromethylbenzyl Phosphate

There total 4 articles about Diethyl-α-trichloromethylbenzyl Phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.3%

Diethyl-α-trichloromethylbenzyl Phosphite (100142-13-0) → Diethyl-α-trichloromethylbenzyl Phosphate (72945-89-2)

Guidance literature:

With iodine; dimethyl sulfoxide; In chloroform; at 20 ℃; for 20h;

Reference yield:

diethyl chlorophosphate (814-49-3) + 2,2,2-trichloro-1-phenylethanol (2000-43-3) → Diethyl-α-trichloromethylbenzyl Phosphate (72945-89-2)

Guidance literature:

With triethylamine; In benzene; at 35 - 40 ℃; for 1h;

Reference yield:

2,2,2-trichloro-1-phenylethanol (2000-43-3) → Diethyl-α-trichloromethylbenzyl Phosphate (72945-89-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 69 percent / triethylamine / diethyl ether

2: 43.3 percent / dimethyl sulfoxide, iodine / CHCl₃ / 20 h / 20 °C

With iodine; dimethyl sulfoxide; triethylamine; In diethyl ether; chloroform;

upstream raw materials:

tetrachloromethane

triethyl phosphate

benzaldehyde

Diethyl-α-trichloromethylbenzyl Phosphite