N-((1S,2R)-2-(3-pyridinecarboxamido)cyclohexanecarboxyl)-2,3,4-tri-O-acetyl-α-L-fucopyranosylamine

Base Information

• Chemical Name: N-((1S,2R)-2-(3-pyridinecarboxamido)cyclohexanecarboxyl)-2,3,4-tri-O-acetyl-α-L-fucopyranosylamine
• CAS No.: 1242140-32-4
• Molecular Formula: C₂₅H₃₃N₃O₉
• Molecular Weight: 519.552
• Mol file: 1242140-32-4.mol

Synonyms:N-((1S,2R)-2-(3-pyridinecarboxamido)cyclohexanecarboxyl)-2,3,4-tri-O-acetyl-α-L-fucopyranosylamine

Chemical Property of N-((1S,2R)-2-(3-pyridinecarboxamido)cyclohexanecarboxyl)-2,3,4-tri-O-acetyl-α-L-fucopyranosylamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-((1S,2R)-2-(3-pyridinecarboxamido)cyclohexanecarboxyl)-2,3,4-tri-O-acetyl-α-L-fucopyranosylamine

There total 2 articles about N-((1S,2R)-2-(3-pyridinecarboxamido)cyclohexanecarboxyl)-2,3,4-tri-O-acetyl-α-L-fucopyranosylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

nicotinic acid (59-67-6) + C19H30N2O8 → N-((1S,2R)-2-(3-pyridinecarboxamido)cyclohexanecarboxyl)-2,3,4-tri-O-acetyl-α-L-fucopyranosylamine (1242140-32-4)

Guidance literature:

With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; In dichloromethane; at 20 ℃; for 18h;

DOI:10.1016/j.carres.2010.03.012

Reference yield:

nicotinic acid (59-67-6) + C19H29NO9 → N-((1S,2R)-2-(3-pyridinecarboxamido)cyclohexanecarboxyl)-2,3,4-tri-O-acetyl-α-L-fucopyranosylamine (1242140-32-4)

Guidance literature:

With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; In dichloromethane; at 20 ℃; for 18h; Inert atmosphere;

DOI:10.1039/c1ob05573a

Reference yield: 95.0%

N-((1S,2R)-2-(3-pyridinecarboxamido)cyclohexanecarboxyl)-2,3,4-tri-O-acetyl-α-L-fucopyranosylamine (1242140-32-4) → N-((1S,2R)-2-(3-pyridinecarboxamido)cyclohexanecarboxyl)-α-L-fucopyranosylamine (1242140-23-3)

Guidance literature:

With methanol; sodium methylate; at 20 ℃; Inert atmosphere;

DOI:10.1039/c1ob05573a

upstream raw materials:

nicotinic acid

Downstream raw materials:

N-((1S,2R)-2-(3-pyridinecarboxamido)cyclohexanecarboxyl)-α-L-fucopyranosylamine