N-phenyl-α,α-dideuteriobenzenemethanamine

Base Information

Chemical Name:N-phenyl-α,α-dideuteriobenzenemethanamine
CAS No.:136295-03-9
Molecular Formula:C₁₃H₁₃N
Molecular Weight:185.237
Hs Code.:

Synonyms:N-phenyl-α,α-dideuteriobenzenemethanamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-phenyl-α,α-dideuteriobenzenemethanamine

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Technology Process of N-phenyl-α,α-dideuteriobenzenemethanamine

There total 21 articles about N-phenyl-α,α-dideuteriobenzenemethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 21175-64-4
1,1-dideuteriophenylmethanol

: 62-53-3
aniline

: 136295-03-9
N-phenyl-α,α-dideuteriobenzenemethanamine

Guidance literature:: With cesiumhydroxide monohydrate; oxygen; In 1,3,5-trimethyl-benzene; at 140 ℃; for 24h;
DOI:10.1002/ejoc.201500086

Reference yield: 94.0%

: 21175-64-4
1,1-dideuteriophenylmethanol

: 587-03-1
3-methylbenzyl alcohol

: 62-53-3
aniline

: 75366-13-1
N-(3-methylbenzyl)aniline

: 136295-03-9
N-phenyl-α,α-dideuteriobenzenemethanamine

Guidance literature:: With 2,2,4,4,6,6-hexachloro-1,3,5-triaza-2,4,6-triphosphorine; In 1,2,4-Trimethylbenzene; Inert atmosphere;
DOI:10.1002/chem.201102446

Reference yield: 87.0%

: 93-98-1,5705-51-1
N-phenyl benzoyl amide

: 136295-03-9
N-phenyl-α,α-dideuteriobenzenemethanamine

Guidance literature:: With [bis(2-methylallyl)cycloocta-1,5-diene]ruthenium(II); dideuterioformic acid; bis(trifluoromethanesulfonyl)amide; triethylamine; [2-((diphenylphospino)methyl)-2-methyl-1,3-propanediyl]bis[diphenylphosphine]; In dibutyl ether; at 130 ℃; for 24h;
DOI:10.1002/adsc.201900406