allyl O-<2-O-benzoyl-4,6-di-O-benzyl-3-O-(tetrahydro-2-pyranyl)-β-D-glactopyranosyl>-(1<*>3)-2,4,6-tri-O-benzyl-α-D-galactopyranoside

Base Information

• Chemical Name: allyl O-<2-O-benzoyl-4,6-di-O-benzyl-3-O-(tetrahydro-2-pyranyl)-β-D-glactopyranosyl>-(1<*>3)-2,4,6-tri-O-benzyl-α-D-galactopyranoside
• CAS No.: 106238-72-6
• Molecular Formula: C₆₂H₆₈O₁₃
• Molecular Weight: 1021.21

Synonyms:allyl O-<2-O-benzoyl-4,6-di-O-benzyl-3-O-(tetrahydro-2-pyranyl)-β-D-glactopyranosyl>-(1<*>3)-2,4,6-tri-O-benzyl-α-D-galactopyranoside

Chemical Property of allyl O-<2-O-benzoyl-4,6-di-O-benzyl-3-O-(tetrahydro-2-pyranyl)-β-D-glactopyranosyl>-(1<*>3)-2,4,6-tri-O-benzyl-α-D-galactopyranoside

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Technology Process of allyl O-<2-O-benzoyl-4,6-di-O-benzyl-3-O-(tetrahydro-2-pyranyl)-β-D-glactopyranosyl>-(1<*>3)-2,4,6-tri-O-benzyl-α-D-galactopyranoside

There total 1 articles about allyl O-<2-O-benzoyl-4,6-di-O-benzyl-3-O-(tetrahydro-2-pyranyl)-β-D-glactopyranosyl>-(1<*>3)-2,4,6-tri-O-benzyl-α-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

allyl 2,4,6-tri-O-benzyl-α-D-galactopyranoside (61236-87-1) + Benzoic acid (2R,3S,4S,5S,6R)-5-benzyloxy-6-benzyloxymethyl-2-chloro-4-(tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-3-yl ester (81726-72-9) → allyl O-<2-O-benzoyl-4,6-di-O-benzyl-3-O-(tetrahydro-2-pyranyl)-β-D-glactopyranosyl>-(1<*>3)-2,4,6-tri-O-benzyl-α-D-galactopyranoside (106238-72-6)

Guidance literature:

With silver trifluoromethanesulfonate; tetramethylurea; In dichloromethane;

DOI:10.1016/0008-6215(86)80014-3

Reference yield: 97.0%

allyl O-<2-O-benzoyl-4,6-di-O-benzyl-3-O-(tetrahydro-2-pyranyl)-β-D-glactopyranosyl>-(1<*>3)-2,4,6-tri-O-benzyl-α-D-galactopyranoside (106238-72-6) → allyl O-(2-O-benzoyl-4,6-di-O-benzyl-β-D-galactopyranosyl)-(1<*>3)-2,4,6-tri-O-benzyl-α-D-galactopyranoside (106284-64-4)

Guidance literature:

With water; In methanol; acetic acid; at 100 ℃; for 1h;

DOI:10.1016/0008-6215(86)80014-3

Reference yield: 97.0%

allyl O-<2-O-benzoyl-4,6-di-O-benzyl-3-O-(tetrahydro-2-pyranyl)-β-D-glactopyranosyl>-(1<*>3)-2,4,6-tri-O-benzyl-α-D-galactopyranoside (106238-72-6) → allyl O-(4,6-di-O-benzyl-3-O-(tetrahydro-2-pyranyl)-β-D-galactopyranosyl)-(1<*>3)-2,4,6-tri-O-benzyl-α-D-galactopyranoside (106238-76-0)

Guidance literature:

With sodium methylate; In methanol; for 6h; Heating;

DOI:10.1016/0008-6215(86)80014-3

upstream raw materials:

allyl 2,4,6-tri-O-benzyl-α-D-galactopyranoside

Benzoic acid (2R,3S,4S,5S,6R)-5-benzyloxy-6-benzyloxymethyl-2-chloro-4-(tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-3-yl ester

Downstream raw materials:

allyl O-(4,6-di-O-benzyl-3-O-(tetrahydro-2-pyranyl)-β-D-galactopyranosyl)-(1<*>3)-2,4,6-tri-O-benzyl-α-D-galactopyranoside

allyl O-(2-O-benzoyl-4,6-di-O-benzyl-β-D-galactopyranosyl)-(1<*>3)-2,4,6-tri-O-benzyl-α-D-galactopyranoside

allyl O-(2,4,6-tri-O-benzyl-β-D-galactopyranosyl)-(1<*>3)-2,4,6-tri-O-benzyl-α-D-galactopyranoside

allyl O-(2,4,6-tri-O-benzyl-3-O-(tetrahydro-2-pyranyl)-β-D-galactopyranosyl)-(1<*>3)-2,4,6-tri-O-benzyl-α-D-galactopyranoside

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