(4-(benzyloxy)phenyl)(2-(2,5-bis(benzyloxy)phenyl)cyclopent-1-en-1-yl)methanone

Base Information

Chemical Name:(4-(benzyloxy)phenyl)(2-(2,5-bis(benzyloxy)phenyl)cyclopent-1-en-1-yl)methanone
CAS No.:1357444-50-8
Molecular Formula:C₃₉H₃₄O₄
Molecular Weight:566.697
Hs Code.:

Synonyms:(4-(benzyloxy)phenyl)(2-(2,5-bis(benzyloxy)phenyl)cyclopent-1-en-1-yl)methanone

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Chemical Property of (4-(benzyloxy)phenyl)(2-(2,5-bis(benzyloxy)phenyl)cyclopent-1-en-1-yl)methanone

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Technology Process of (4-(benzyloxy)phenyl)(2-(2,5-bis(benzyloxy)phenyl)cyclopent-1-en-1-yl)methanone

There total 6 articles about (4-(benzyloxy)phenyl)(2-(2,5-bis(benzyloxy)phenyl)cyclopent-1-en-1-yl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1266452-53-2
8-(benzyloxy)-2,3-dihydrocyclopenta[c]chromen-4(1H)-one

: 1357444-50-8
(4-(benzyloxy)phenyl)(2-(2,5-bis(benzyloxy)phenyl)cyclopent-1-en-1-yl)methanone

Guidance literature:: Multi-step reaction with 3 steps

1.1: water; sodium hydroxide / acetone / 5 h / 65 °C / Inert atmosphere

1.2: 8 h / 50 °C / Inert atmosphere

2.1: 4-methyl-morpholine / toluene / 16 h / 25 °C / Inert atmosphere

3.1: tetrahydrofuran; toluene / 4 h / 0 °C / Inert atmosphere

With 4-methyl-morpholine; water; sodium hydroxide; In tetrahydrofuran; acetone; toluene;
DOI:10.1021/ol203264a

Reference yield:

: 1379614-64-8
2-(2,5-bis(benzyloxy)phenyl)cyclopent-1-enecarboxylic acid

: 1357444-50-8
(4-(benzyloxy)phenyl)(2-(2,5-bis(benzyloxy)phenyl)cyclopent-1-en-1-yl)methanone

Guidance literature:: Multi-step reaction with 2 steps

1: 4-methyl-morpholine / toluene / 16 h / 25 °C / Inert atmosphere

2: tetrahydrofuran; toluene / 4 h / 0 °C / Inert atmosphere

With 4-methyl-morpholine; In tetrahydrofuran; toluene;
DOI:10.1021/ol203264a

Reference yield:

: 611-10-9
2-ethoxycarbonyl-1-cyclopentanone

: 1357444-50-8
(4-(benzyloxy)phenyl)(2-(2,5-bis(benzyloxy)phenyl)cyclopent-1-en-1-yl)methanone

Guidance literature:: Multi-step reaction with 5 steps

1.1: methanesulfonic acid / 72 h / 30 °C

2.1: potassium carbonate; sodium iodide / acetone / 18 h / Reflux; Inert atmosphere

3.1: water; sodium hydroxide / acetone / 5 h / 65 °C / Inert atmosphere

3.2: 8 h / 50 °C / Inert atmosphere

4.1: 4-methyl-morpholine / toluene / 16 h / 25 °C / Inert atmosphere

5.1: tetrahydrofuran; toluene / 4 h / 0 °C / Inert atmosphere

With 4-methyl-morpholine; methanesulfonic acid; water; potassium carbonate; sodium iodide; sodium hydroxide; In tetrahydrofuran; acetone; toluene;
DOI:10.1021/ol203264a